Tag Archives: Natural dyeing

the conserved Bacton Altar cloth.

Queen Elizabeth I dress (The Bacton Altar Cloth)

By Ashley Walker
Copyright 24th February 2020

Inner courtyard of Hampton Court Palace with Henry 8th Great hall on left.

We saw the social media posts about this 400 year+ old textile and noted the brightness of the green embroidery silks. Unusual we thought. The longest lasting green dyes are combinations of a yellow dye with indigo. Indigo we know can last for many centuries but what was the yellow dye? Most yellow and green natural dyes do not last long and old textiles end up in various shades of blue (from indigo), red (from madder or an insect dye) and brown from all the other dyes which have faded.

blue and red the only colours to survive on old tapestries

This is one of the many rich tapestries from Hampton Court Palace. Typical of tapestries of this age, only the blue and red dyes have survived.

We arranged with a friend to go and see the dress at Hampton Court Palace. Where colour is concerned you really need to see it with your own eyes. There were some disappointments on our way there, notably the cost of getting into the Palace – ouch! Then there was the ‘No photography’ policy and the general lack of information available on the textile’s construction. No souvenir leaflet or postcard to take away or purchase either. According to one red-coated guide, the owners of the textile (the local diocese of the Church of England) had insisted that no financial gain was allowed through merchandise. As it turned out the palace guides were not enforcing the No Photography policy in any way, so I was able to get some good pictures.

Unfortunately the reverse side of the fabric, which has the brightest colour, was not on show but the faded side was still quite colourful and the greens still discernible.

For a general history of the textile, look at the links at the bottom of this post. The articles are highly recommended. We were impressed by the skill and artistry of the original embroiderer. This master craftsperson had embroidered the entire design straight onto the cloth of silver. The plant based motifs may have been inspired by illustrations from a Herbal (a contemporary plant guide) but could also have come from other textiles of the period. Many of the plant motifs are entirely recognizable and have been worked with a fine outline and fill of very closely spaced “seed stitch”. At some point additional, embroideries were added to the dress but these are of much lesser quality and were, according to historians, done by Court noblewomen. This secondary work consists of various animals, many of which are insects. Caterpillars are particularly common. These animals, and the odd tree, were placed in the white areas between the plant motifs, seemingly at random. This lead to a rather chaotic appearance, which to my eye, spoiled the entire design. I would not be surprised if this “fault” had resulted in the fabric’s survival. Just picture the scene – Elizabeth is shown the reworked dress and notes its chaotic design. She smiles and says “thankyou ladies that’s just lovely”. Then as soon as they are gone she thinks “Oh, what can I do with it now, I can’t give it to anyone in court as it’s just too opulent, I know, I’ll send it away up north as a remembrance gift for my lady companion Blanche Parry. That way it will never be worn again”. That’s the beauty of history, you can fit any story you like to the facts.

Detail of the Bacton Altar Cloth showing floral and animal motifs. The greens and yellows on this faded side of the textile retain some of their colour, probably the result of being kept out of direct sunlight in a church for 300+years.

without the animal embroideries the design is much nicer

I have photoshopped this to show the textile as it might have appeared without the extra animal embroideries.

Portrait of Elizabeth 1st wearing a similar dress

This highly symbolic portrait of Elizabeth shows her wearing a dress of similar design to the lost dress.

Borago officinalis

So, what about the dyes used in the dress? After searching the internet, the only dyes mentioned are cochineal from Mexico and indigo from the far east. This means the blue probably comes from from Indigofera. The silk cloth (Cloth of silver) itself was probably sourced in Italy, so it is likely that the dyed embroidery thread was also sourced from abroad, which opens up the dye possibilities enormously. I would not be surprised to learn that the master embroiderer was also European, rather than English.

I have enquired with the conservators at Hampton Court about the dyes used, but as yet I have not had a reply. However, I have been in contact with Natalie Walker (no relation) who has done some research on this textile and tells me the chief conservator at Hampton Court will be publishing a paper on the subject soon. If I find out any more I will update this blog with the results.

The visit to Hampton Court Palace was a timely reminder of what can happen when extreme wealth and power is held in the hands of a tiny group of people. Queen Elizabeth II is still the official owner of the Palace.

Note: All the photos in this post were taken by the author.

See very good posts by Natalie Walker, Hampton Court and the Crown Chronicles on the Bacton Altar Cloth here:

A Mark of Craftsmanship?

https://www.hrp.org.uk/hampton-court-palace/whats-on/the-lost-dress-of-elizabeth-i/#gs.xdatlg

The Bacton Altar Cloth – Elizabeth I’s only surviving dress – now at Hampton Court Palace

Madder red and indigo bluedyed handspun and knitted jumper

From fleece to jumper in 6 years

By Ashley Walker
Copyright 11th February 2020

Ever since starting to grow our own dye plants I have wanted to create something I could wear, something that had been created from scratch. In the past I have been quite content to use bought materials to create works of art and craft but as I got older this has appealed less and less. I used to be confused by people who wanted to go back to creating the raw materials of their crafts. I thought that the raw materials were just tools to aid creativity and it was easy to buy the best. I never concerned myself about where they came from or how they had been produced. In time something changed and the thought of creating the raw materials myself began to be more important. I do not really understand the reasons why.

Growing our own dye plants was at first a sort of curiosity but one that propelled us into the world of spinning fleece. After all if you are prepared to grow your own dyes then it no longer seems right to use them to dye commercially manufactured textiles. What would be the point of that? So fleeces were obtained and Susan set out on the road of learning how to clean and mordant them. Later came carding, spinning (drop spindle and wheel) and plying into yarn with diversions into weaving and peg loom weaving. But learning all the steps to achieve a finished dyed garment has turned out to be a steep hill to climb.

Once I had learned how to spin I decided to dye sufficient fleece to make a jumper and trusted to my ability to learn how to knit when I had enough yarn.

Red madder dyed fleece being carded into rollags and spun into yarn

Red madder dyed fleece being carded into rollags, spun and wound into balls ready for knitting

The first photo I have of the beginning was taken in 2014 and shows some of the madder dyed fleece and yarn. However by the time this was taken I had probably been at it for quite a while. The dyeing process was done very carefully so as not to felt the wool. Chopped root was heated to about 60ºC and the fleece added. The dye pans were then placed in a hay box and left overnight. The next day the fleece would be removed and the chopped root at the bottom of the pan was pounded to help release more alizarin (the chief red dye of madder). The pot was then reheated and fleece reintroduced. This might be repeated 3 or more times before a suitable red was obtained.

Slowly, slowly I built up a good stock of dyed fleece to spin. The shades of red varied so I tried to blend the darkest with the lightest to obtain as even a result as possible. Even so the yarn shows a variation in colour which results in the very pleasing stripes of the finished jumper.
Once I had enough I needed a knitting pattern and I quickly found out that knitting patterns are created for consistently even commercial yarn, not home-spun. But with help from our good friend Brian Bond and a few test squares of my own knitting I ended up with a ‘sort of’ pattern I thought I could work to. This was adapted from a cardigan design in one of Brian’s books that I liked the look of. But that’s where it all came to a bit of a grinding halt. I started on the indigo dyed blue rib of one side of the jumper but after several weeks of trial, with much undoing I had barely got into the red. The level of concentration needed to knit was so great that the slightest distraction caused dropped or added stitches or some other mistake. Even when I thought I was concentrating I would often find myself knitting the wrong stitch and all this before I had got to the point of having to reduce the number of stitches or do any of the fancy edging. It was too much.

shows blue rib and a bit of the red dyed yarn knitted on circular needles

This is as far as I was able to take it on my own.

The wool and the bit of rib stayed in its bag for months until Susan took pity on me and decided to have a go herself. Susan can knit but has no experience of knitting with irregular yarn. So what did get knitted took a long time and wasn’t remotely the right shape or size. Susan was canny enough to know that sewing the pieces together would have resulted in an unusual jumper to say the least. So back into its bag it went. Then along came Tracey Ballard who said nonchalantly “Oh yes I’ll finish that off for you if you like”. It meant that my dream of doing it all myself was truly out the window but by this time I was a pushover to accept any help.

No doubt after much remedial work (we suspect more than has been admitted to) Tracey turned up with the finished jumper a few months later. It was exactly as I imagined it. It is heavy and warm and it fitted perfectly. It is the first new jumper I have worn since one my mum knitted me many years ago. I failed to do it all myself but the feeling when wearing it… well it’s indescribable. The colour red is bold and bright. Red was my fathers’ favourite colour. He would buy me red shirts for Christmas which I would never wear. Now I have a totally unique red jumper, one that could never be bought in a shop and one that I will be proud to wear and show off for the rest of my life. No doubt my Dad would have approved.

Ashley wearing the newly delivered jumper

The smile says it all.

Thanks to Susan and Brian for encouragement and advice. Special thanks to Tracey for finishing it off. It is friends and the small things that make life worth living even if they do take 6 years to complete.

shows rear of red madder dyed jumper with red stripes - the result of uneven dyeing

The back of the jumper showing the stripes produced by variations in the dye.

A monster in the greenhouse

Growing American Pokeweed in the UK
Phytolacca americana

By Ashley Walker
Copyright 20th January 2020

First a warning. All parts of this plant are poisonous to humans and most animals except birds. It is also invasive so its growing must be carefully controlled.

I had heard a lot about this controversial dye plant, but in the UK it’s still much of a novelty. So when I spotted some plants growing in a greenhouse nursery in Devon in 2018 I “obtained” a berry containing a few seeds. I grew them last year (2019) just to see for myself what all the fuss was about.

Horticulture

Three of my seeds sown in April germinated after about 2 weeks.

shows the baby seedlings growing in a seed tray

The three seedlings of American Pokeweed showing seed leaves and red stems

shows size of plant by late June already getting big and lush

By June the plant in the greenhouse was already looking like a lush spinach plant.

The pink stemmed seedlings were very vigorous and had to be potted on after a few weeks. By the time I judged it was warm enough to plant out in May/June the plants were already around 10in high. My first observation was how similar they look to our native Deadly Nightshade (Atropa belladonna) despite belonging to a totally different plant family. Pokeweed is sometimes called American Nightshade and I think this is not just because of its toxic qualities.

Not taking any chances with late frosts I planted one of the plants in our greenhouse and the other two outside in the garden. The plant in the greenhouse grew with extraordinary rapidity, its reddish stem swelling out to more than 2 inches in diameter. By the Autumn it had escaped through the window in the greenhouse roof reaching 7ft. An extraordinary “triffid” of a plant!  Outdoors the plants did not do so well only growing to about 4ft.

The pokeweed plant was so vigorous it had escaped through the greenhouse window

By October the plant had escaped though the greenhouse window and was threatening to take over the whole greenhouse.

Closeup shot of American Pokeweed flower spike

The pink flower stems are quite attractive.

The berries of American Pokeweed start as green then turn pink and finally black at which point they are ready to be used to dye.

Shows a different variety of Pokeweed with short clublike raceme of green berries.

This photo shows the other variety of Pokeweed with short “club like” racemes of berries. Spotted growing at Bell House.

A Large American Pokeweed plant growing in the Hornimams museum dye plant garden showing upright short racemes of ripe berries

A slightly out of focus shot of the mature American pokeweed plant growing in the Horniman’s museum dye plant garden showing short upright racemes of ripe berries.

There are several cultivars of pokeweed available commercially – the chief difference between them appears to be the shape of the flower and berry racemes. In one type the racemes are short, upright and club-like (sometimes given a separate species name P. rigida) and in the more decorative type they are long, thin and pendulous. The plant is a herbaceous perennial native to North America which can reach 10ft in a single season before dying back to the ground during the winter.

Our variety is the one with long thin pendulous racemes. Later in the year we found plants of the other variety growing at the Horniman museum dye garden in Forest Hill, South London and in the gardens at Bell House, Dulwich. At Bell house it grows as a weed which demonstrates how invasive it can be.

Dyeing Method

Once the berries had ripened and turned black I picked a few racemes and test dyed on a small piece of alum mordanted wool yarn. Internet advice indicates that the best method is to make a dye bath from several times the weight of fibre to be dyed in berries, heated with the strongest acetic acid you can get hold of. I had some 10% acetic acid left which I bought to fumigate an old bee hive. At this strength the vapour alone can rust steel so caution is required. Distilled white vinegar is probably the next best thing. The yarn quickly took a very pleasing bright red colour (much quicker and easier than madder) but the big question was how long would it last? Some dyers say it can last years and others say it fades within a matter of weeks. I hung up my sample in the window with half of it covered in foil to keep the light out.

Light fastness

After about 80 days I took it down and had a good look at it. The wool exposed to the daylight had indeed faded with the side facing the outside more faded than the side facing inwards. What is more the red is fading to a disappointing brown (in the photo it looks more orange than it actually is). The window is incidentally a north facing one so it would presumably fade even quicker in direct sunlight. The covered part of the sample still shows a good red. From experience of other fugitive plant dyes I would guess that textiles dyed with pokeberry could be made to last a few years if kept in the dark and only worn intermittently indoors. But I’m not sure it’s worth it. When freshly dyed the colour is fabulous and I’m sure that when the native Americans used it to dye their ponies they made a glorious (and terrifying) sight. But coupled with the potential hazards of growing the plant I think that its continued inclusion in our dye garden is in the balance. Susan is all for eradicating it immediately so it’s on borrowed time!

Light fast test yarn showing fading of red to brown

The upper part of this wool yarn sample was exposed to light in a North facing window for 80 days. The lower part which was wrapped in foil remains a good red while the exposed part has faded to brown (in this photo brown looks more orange than it really is.

The same yarn from an indoor photo showing the side of the yarn that was facing the window which shows more fading

This photo (taken indoors shows the side of the yarn that was facing the window which has suffered the most fade.

This side of the wool yarn was facing inwards and has suffered less fade. The bottom part was covered in tin foil and has suffered little or no fade.

Conclusions

The plants growing outside managed to resist light frosts but have since died back to the ground. By January the plant protected from the frost in the greenhouse still has green leaves. Information on the web says that the plant mainly reproduces by seed (which can remain fertile for 50 years) but it can also shoot from the roots. There is no doubt that my greenhouse plant has produced many long side roots and the plant is clearly making a bid to take over the whole thing. No doubt the phenomenal growth uses up a lot of soil nutrients too.

On balance I think that where pokeweed grows wild (in North America) and berries can be obtained in quantity via foraging, it can be a fast, fugitive and fun plant dye, but as a dye plant in the UK it’s probably not worth planting it, not when a good permanent red can be got from madder.

Additional information on Pokeweed can be found here:

https://www.fs.fed.us/wildflowers/plant-of-the-week/phytolacca_americana.shtml

http://www.efloras.org/florataxon.aspx?flora_id=1&taxon_id=220010427

https://ucanr.edu/blogs/blogcore/postdetail.cfm?postnum=27983

Horniman Museum Dye Garden:

Formal layout of the Hornimans plant dye garden

The Horniman museum Dye Plant Garden is well worth a visit.

 

https://www.horniman.ac.uk/get_involved/blog/planting-our-dye-gardens

Bell House Gardens:

https://www.bellhouse.co.uk/blog/2019/6/12/perfectly-picturesque-bell-house-garden-in-the-18-th-century

American Pokeweed berries beginning to ripen.

The Natures Rainbow Garden

Would you like to take part in a Nature’s Rainbow “Pilot” Workshop on Planning a Dye plant garden?

Planning and Planting a Dye Plant Garden

UPDATE 9 May 2019
Thank you everyone! We have been overwhelmed by the interest shown in this first pilot workshop.  If you would like to be added to a waiting list in case anyone drops out, or if you would like us to alert you about future courses, please get in touch.

We will post about how the workshop goes after 1st June.

_________________________________________________________________________

Saturday 1st June 2019, 1 – 5pm

Creating a planting plan for beginner dye gardeners, with tips from Susan and Ashley of Nature’s Rainbow. What plants to grow, when to plant, when to harvest, how to maintain the garden.

We have been growing and using dye plants in the historic town of Hitchin for over 14 years.
Help us to design future workshops to share our expertise.

5 places available. Contact us via this blog for further details and how to book.
£20 nominal fee required in advance to confirm your place.

This is a very reduced rate to recognise the fact that the views and feedback from the people attending will be helping to design a future workshop for Nature’s Rainbow.

Participants will have a tour of an established dye garden (as featured in The Journal of Weavers Spinners and Dyers https://www.journalwsd.org.uk/article/the-dye-plant-garden and hear how we manage the mix of annual, biennial and perennial plants within the constraints of our site. We’ll structure the session loosely, so we can maximise the flow of info between us all.

Seeds and perennial root cuttings of madder and small dyer’s broom plants to take away.

In exchange, you need to be willing to provide feedback and ideas on how to design future workshops and bring a simple sketch of your growing space, marking up sunny and shady areas and soil type.

Our house and dye garden is a very short walk from Hitchin Station, with frequent services on the Great Northern train line between Kings Cross, Cambridge and Peterborough.  Please contact us

Susan and Ash

Persicaria tinctoria indigo extraction experiment

Hot vs Cold indigo extraction from fresh Japanese Indigo leaves

By Ashley Walker
Copyright 6th August 2018

Currently the main method of indigo extraction in use on internet Facebook pages is the 2 -3 day long soak in water. I believe this was the main method used commercially in the days before synthetic indigo wiped out the western market for natural indigo. Originally used to extract indigo from Indigofera tinctoria it is still used for small scale production in South Asia. The method is now used for Japanese indigo presumably because the traditional Japanese Method of composting the leaves is too large scale and time consuming for craft dyers. So it has been with some bafflement that I’ve seen the rise of this soaking method as I have always followed the Jenny Dean method which is even quicker.

We were introduced to plant dyeing through the pages of Jenny Dean’s “Wild Colour” and have used her recipe from this book for many years. It involves heating the leaves and can be done in two hours. Since we started to use this recipe we have tweaked it somewhat, discovering that there is no need to heat the leaves over 75 to 80°C to get maximum extraction. Another wrinkle is the need to allow the heated leaves to cool fairly rapidly. Large containers holding 20+ litres tend to cool too slowly and the indigo can be damaged. We did try one experiment when we cooled the extraction bath artificially but that was too quick and the results were very poor. An ideal extraction would be to heat about 1kg of leaves in 5 to 10 litres of water to 75°C and allow it to cool naturally over an hour. In our climate it will fall to around 40°C or less during that time.

So, now to the experiment which was a bit slap dash, but I am sure that it was systematic enough to have fairly good validity for a home dyer.

I picked just over 2kg of fresh Japanese Indigo of the Long Leaf variety which was showing no signs of any flower buds. This was divided into 2 lots of 1026g.

Persicaria tinctoria

Long Leaf Japanese Indigo showing leaf curl – a result of prolonged hot sunny weather.

Hot Soak Method (based on Jenny Dean)

Once batch of leaves was added to a large pan with about 8 litres of cold tap water (20°C) and then gradually heated with constant stirring to 75°C. This took exactly one hour and at the end the leaves had lost all of their fresh green tint and had turned almost black. The water was a very dark grey (a lot darker than usual in fact and I attribute this to a higher than normal amount of indigo in the leaf – a result of the weeks and weeks of hot sunny weather we have had this summer).

The leaves were then left to soak for one more hour, after which there was an indigo bloom at the surface and the water had darkened further. The leaves were removed (by straining through old tights) and 4 tablespoons of household ammonia were added with an immediate colour change to dark yellow/green. The liquid was then oxygenated by pouring from bucket to bucket about 20 times during which the liquid darkened to a green black. A small quantity of the liquid (viewed from above in a white plastic cup) looked olive green.

Indigo extraction from Japanese Indigo Hot and cold methods

Comparison of Hot and cold indigo extraction after 1 hour of soaking but before straining.

Cold Soak Method

The second batch of leaves was placed in a plastic bucket filled with about 8 litres of hot tap water (57°C). I used hot water because I did not wish to wait more than 24 hours. At this temperature the leaves become slightly cooked and release cell contents into the water quicker. The bucket was then set aside for 24 hours. After 1 hour the temperature had fallen to 44°C, the leaves were still quite green and the liquid was much paler and bluer than the hot extraction at the same stage. See image above.

After 24 hours the leaves were still greenish, although they had darkened somewhat. There was a lot of indigo scum on the top leaves. The liquid was grey with a blue tint. The plastic bucket was stained blue. Generally the results so far looked good, with much more blue visible than in the Jenny Dean method.

Indigo extraction from Persicaria tinctoria

Cold indigo extraction after 24 hours. Lots of indigo bloom on leaves.

Indigo extraction from Persicaria tinctoria

After leaves are removed, alkali (ammonia) added and liquid aerated.

Extraction of indigo from Persicaria tinctoria

Comparison of colour of water after extraction.

Leaves of Persicaria tinctoria after indigo extraction.

Colour of leaves after cold soak for 24 hours.

 

Indigo stained bucket

Empty plastic bucket used for 24 hour cold soak now stained with indigo.

The leaves were removed and about 4 tablespoons of household ammonia were added and the colour immediately changed to yellow green. The liquid was then oxygenated, by pouring back and forth between buckets about 20 times. During this process the liquid darkened until it was nearly black. A small quantity looked blue/green.

Dye test

Both extracts were then heated at the same time in separate pans to 50°C, the ideal temperature for dyeing wool, and spectralite reducing agent (thiourea dioxide, thiox) was added (one and a half teaspoons) to each pan. They were then left for about 2 hours to give ample time for the indigo to be reduced. The pots were then reheated to 50°C and an identical skein of wool (Corriedale) was added to each. Both pots were then gently stirred to promote even dyeing and the skeins were removed after 20 minutes.

Results

Initially the colour of the skein from the Jenny Dean (hot) method looked darker but on drying no difference could be detected.

Dye test. hot and Cold extracted indigo from Persicaria tinctoria

Test dye showing relative strengths of dye bath from Hot and Cold extracted indigo.

Conclusions

The amount of indigo extracted appears to be the same for both methods. However, heating, cooking and stirring the leaves increased the amount of fine particulate plant material in the liquid which increased the amount of sludge in the bottom of the dye bath.

I should clarify I don’t use lime (as a combined alkali and flocculating agent) to obtain a dried indigo pigment from my dyeplants. Any indigo I don’t use straightaway for dyeing, I store as liquid sludges. But I can see that for people who do use lime, the cold soak is advantageous because the resulting indigo pigment would contain fewer impurities than the hot soak because the liquid extract after straining is purer. For myself I’m quite happy to continue using my modified Jenny Dean process as it is fast and reliable.

Postscript

Out of interest I also decided to compare the Long Leaf Japanese Indigo to Woad. I processed a similar quantity of Woad leaf according to the 24 hour soak method in the experiment. Another wool skein was dyed in nearly identical conditions and the results prove to me that Woad can actually produce more indigo than Long Leaf Japanese Indigo.

Wool dyed with indigo extracted from Persicaria tinctoria and Isatis tinctoria

Comparison of strength of indigo extracted from Long Leaf  Japanese Indigo and Woad.

A note on alkalis

There has been a lot of controversy about which alkalis produce the best results. I have tried most of them and found that what is important is the pH not the exact chemical used to get there. Washing soda is the weakest and produces very poor results. Household ammonia is excellent and relatively safe, provided you don’t get it on your skin or breathe it in. Calcium hydroxide (lime) is good and has the added benefit of soaking up the indigo precipitate and settling it to the bottom fast (flocculation). Sodium hydroxide is also good but is very corrosive – a danger to skin and textile.
Whenever using strong alkalis you must take safety precautions: wear gloves; avoid splashes; don’t ever add water to dry alkaline powders or granules, add the powder to water; label colourless solutions and store safely; never leave sodium hydroxide solutions unattended for curious animals or children to explore (it is colourless and odourless and very corrosive indeed).

References

Wild Colour by Jenny Dean

Susan Dye and Ashley Walker

The Natures Rainbow garden 2018 – Part one

by Ashley Walker
Copyright August 2018
Banner photograph copyright Sharon Cooper

On the 9th August, after two months with barely a drop of rain, the heatwave and drought in the South East of England may finally have come to an end. Despite regular watering the unnatural weather has taking its toll on our dye plants. For the first time our woad plants are being eaten by Cabbage White butterfly caterpillars (Large White Pieris brassicae and Small White Pieris rapae) and more recently by flea beetles (genus Phyllotreta). I guess the critters were getting desperate to find plants with a bit of juice in their leaves. The weather is having an impact on me as well, I have to water the indigo nearly every day and keeping the rest of the garden needs water too so I’m spending hours each week that I’d rather be spending on writing or dyeing.

This is the first part of a two part post on observations of the dye plants in our garden. This one deals with the plants we have been growing for more than a year. The second part will cover new plants.

European Woad – Isatis tinctoria

Isatis tinctoria being eaten by Large White butterfly caterpillars

These Large White caterpillars managed to eat the whole woad leaf, leaving only the midrib behind.

We have grown Woad for about 12 years now and for the first time our plants have been attacked by caterpillars and flea beetles. This makes a change from the usual small black slugs which put a few holes in the leaves but seldom do any serious damage.

Isatis Tinctoria leaf with eggs and lava of Large Cabbage White butterfly

A cluster of Large White butterfly eggs on the underside of a woad leaf

Isatis Tinctoria being attacked by Flea Beatles

Shiny black small Flea Beatles can slowly chew their way through a woad leaf leaving it like a sieve.

Isatis tinctoria

Woad flower spike August 2018 – from seed to flower in one season as a result of pampering.

I expect that the extraordinary hot weather is to blame with the butterflies and beetles probably acting in desperation. Although the flea beetles appear to thrive, the caterpillars have had a much harder time digesting the unpalatable leaves and most of the newly hatched critters have simply died, leaving a few small holes in the leaf. Only one plant had its leaves reduced to its midrib but even this one will survive as it is now putting out new growth. Interestingly it appears to be only the plants I have watered which are being eaten. There are a few plants which never get watered and these are looking fine.

A few people have asked about growing Woad in tubs or containers and this year we’ve had a few in containers ourselves and this has revealed a problem. One of our plants grown in a container in good compost and watered and fed regularly has grown large and is currently putting out a flower spike which will drastically reduce the amount of indigo in its leaves. Its very unusual to see Woad flowering in August so I can only assume we have pampered it too much – given it the ability to grow large enough to flower in one season. So if you are growing Woad in containers don’t give them too much fuss!

Chinese Woad – Isatis indigotica  

Isatis indegotica

Chinese Woad – about as big as it gets before flowering

Isatis indigotica

Planted out in April these Chinese Woad immediately produced flower stems

We have been growing this for two years now, desperately trying to find out how to stop it flowering a few months after planting. From what I’ve read I’m in good company and this is the chief reason Chinese Woad has not caught on as a source of indigo, despite the fact that it could potentially produce as much dye as Japanese Indigo. Some of the literature indicates that botanists think Isatis indigotica is basically just a variety of tinctoria (European Woad). However, if that is so it has evolved away from tinctoria to a considerable extent. Indigotica is clearly adapted to a much warmer climate and although still nominally a biennial it behaves much more like a half hardy annual. It will flower at any time of year, even in winter, so its rosette stage is always very short and the plant never gets very big. The leaves are a paler blue-green than European Woad and its yellow flowers will continue to be produced throughout the year provided the plants are watered and taken care of. Once the plant starts to flower the larger rosette leaves die off leaving only small leaves on the plant which are probably no good for dyeing. According to the Handbook of Natural Colorants, indigotica will be triggered into flowering if the night time temperature falls below 5°C, which makes it almost impossible to grow the plant to any respectable size here in the UK. Even in Mediterranean climates the plant can only usefully be grown in the Summer. From my experience the plant will flower even if you just look at it the wrong way so I’m coming to the conclusion that it’s not worth the effort. It does grow very quickly however and if you were to grow it en masse and harvest the leaves before it flowered it might just provide a return for your efforts.

Another problem with Chinese Woad is its susceptibility to pests. Caterpillars and aphids like it very much and can easily destroy your plants.  And you guessed it, significant insect damage will also trigger flowering. In a mad moment I decided to see if Chinese Woad tasted any nicer than European Woad. But the taste test settled nothing, both plants are extremely bitter and fiery. I obviously don’t have the finer tastes of Cabbage White butterfly caterpillars!

Japanese indigo – Persicaria tinctoria

Persicaria tinctoria - Long Leaf variety

Long leaf variety of Japanese Indigo with curled leaves to protect itself the prolonged hot sun of 2018

This year we are growing the same three varieties as last year – Long Leaved, Broad Leaved and an Intermediate Leaved white flowered variety. There appears to have been no interbreeding from last year. This year the difference between the long leaf and broad leaf varieties is stark. The Long Leaf plant is very vigorous with dark green leaves. The Broad Leaf variety took a long time to get going as usual and suffered from its leaves turning red. I was initially confident that the red colour was partly due to the hot sunny weather we were having in early summer – the slow growing plants were getting roasted. But after a good feed (with chicken manure pellets) the plants started growing quickly with the new foliage a nice mid green despite the continued hot sunny weather. So a bit of a chicken and egg situation: was it the lack of fertilizer that caused the leaves to redden or simply that the young plant leaves, growing slowly, were getting a longer exposure to the hot sun?  The Long Leaf variety reacted differently to the hot sun with leaf curling , something I had seen last year but only on plants grown in the greenhouse.

Persicaria tinctoria

A bed of intermediate White flowering Japanese Indigo.

Persicaria tinctoria

Newly planted out Broad Leaf Japanese Indigo with sun reddened leaves.

Thus far we have only harvested the Long Leaf variety and used it in a little experiment comparing Jenny Dean’s extraction technique with the more often used long soak in cool water. The results will be written up in a later post. What I have also noticed is that we are currently getting a considerably better production of indigo from Woad than the Long Leaf variety of Japanese Indigo. Woad is well known for giving better results when the weather is hot and sunny. If the climate change predictions are correct and we continue to have hot summer weather then I think we would be better to return to growing mostly Woad. The Long Leaf variety of Japanese Indigo produces the least amount of indigo dye of the three varieties (see comparison here) but it does produce larger plants so perhaps still produces an equivalent amount of indigo per square metre.

Madder – Rubia tinctorumRubia tinctorum berries

Once again this year the madder plants are producing masses of berries. This is the third year running. In the previous 10 years or so the plants produced only a few. I have no explanation as to why this is.  I’ve grown plants in different soil, in planters and in the ground and all plants are doing the same. A result of the weather?

Rubia tinctorum

Madder plant obtained from Southwark Cathedral in early 2018.

This year we obtained a new madder plant sourced from Southwark Cathedral dye garden. The plant is quite different to plants I have been growing up to now (all of which were derived from a single seed over 10 years ago). This new plant has paler leaves with a different shape and it flowers about 3-4 weeks later. It will be interesting to see if the root yield is also different. I’m pleased to have been able to increase the genetic diversity of our madder as I’ve always propagated by root stem cuttings or from seeds from my own plants.

Wild Madder – Rubia peregrina

Rubia peregrina

Wild Madder in flower – Early July

We’ve been growing this plant for nearly three years now. It’s an evergreen but the tops do not appear to be totally hardy in the UK climate and were damaged by the winter frosts. This is the first year in which the plants (originally obtained from a wild flower nursery) are starting to look a bit happier. They are putting out new shoots from underground stems and flowering for the first time. It remains however a very slow growing perennial and I think it will take longer than Common Madder to produce a good root harvest so we are leaving it for another year.

I was given some seed from a friend from some wild plants growing on the south west coast which nearly all germinated though it did take well over a month before the first shoots appeared.

Saw wort – Serratula tinctoria

Serratula tinctoria

Saw-Wort plants with yellowing of leaves.

Serratula tinctorum

A self seeded plant with dark green leaves growing next to the transplanted ones with yellow leaves.

This native  plant continues to be disappointing. Not only do the plants remain small but about half of them suffer from bad yellowing of the leaves once planted out in the garden. I have tried practically everything to remedy the problem – fertiliser, Epsom salts and seaweed extract. There are some self-seeded plants which look very healthy so I do wonder if the roots are somehow getting seriously damaged during transplanting. It also remains likely that there is something wrong with the soil itself as other plants (Genista, a red scabious and a Purging Buckthorn shrub) are similarly affected.

Serratula tinctoria dye comparison

A comparison of our main yellow dye plants. Top is Weld, Bottom Right is Genista and Bottom Left is Saw-Wort

We did try dyeing with the Saw Wort this year and obtained a good buttery yellow. We were hoping it would be a nice lemon yellow like Weld and Genista so were a bit disappointed with that too.

Dahlia species

Dahlia Species

Bumble bee on single type dahlia grown from seed.

Dahlia Species

Dark Red Dahlia giving pinky purple and greens. Possibly “Nuit d’Ete” or “Black Cat”

The colour of Dahlia flowers has an effect on its dye but we did not appreciate by just how much until this year when we tried using some deep red flowers to dye with. We obtained nothing like our accustomed strong yellows with acid pH and strong orange with alkaline pH. This time we got green with alkali and blue/purple with acid indicating that the dyes in this dark red flower were the same as you find in red cabbage and some other red flowers. These dyes, although very pretty, are not light fast. Over the years of growing Dahlia we have narrowed down the varieties that produce the best results for the home dyer. These are yellow or orange double flowering pom pom types. The pom pom flowers are longer lasting and produce more dye – some pom poms are very large and yield a lot of dye but bees and pollinators are unable to assess the nectaries. We have tried to stay away from these but there’s no doubt they are the best for dyers.

Tansy – Tanacetum vulgare

Tanacetum vulgare

Tansy needs regular watering for healthy plants.

Often used by Scottish dyers as a source of yellow dye this plant has been growing in our garden for several years now but largely unused because the plant wasn’t very vigorous. There was never enough plant material to harvest and the flowers were disappointing. This year we planted a bed of Japanese indigo alongside so the Tansy benefitted from being regularly watered. The resulting Tansy flowers have been lovely so if you’re growing them keep them watered for best results.

Perennial Coreopsis –  Coreopsis grandiflora varieties e.g. Golden Joy, Sun Ray, Early Sunrise

Coreopsis grandiflora

Perennial coreopsis – plant breeders benefitting the plant dyer.

Coreopsis grandiflora

Bright orange on alum mordanted wool blanket.

These are double flowering perennials with deep orangey yellow flowers which produce a lot of dye. They are not as hardy as the growers would have you believe as half our plants died during the winter and only a few have recovered enough to put on a good show this year. However, many can be easily grown from seed so are not too expensive to grow. They make excellent bedding plants and produce a fabulous orange dye from the flowers. An example of the plant breeders unwittingly aiding the home dyer.

Dyer’s Alkanet – Alkanna tinctoria?Alkanna tinctoria

Alkanna tinctoria

Alkanet root. Bottom tip has had thin outer black bark removed revealing the dissapointingly white root.

This is the third year of growing and though I have not tried to extract any dye from its roots I am deeply disappointed to find that the roots are not red as they should be. I was suspicious as soon as I started to grow the plant from seed bought from the German Company Rühlemann’s. The plant seemed too vigorous with over large leaves and not hairy enough, but I persisted with it until it flowered. The flower shoots were tall (up to about a metre high) and not at all like the creeping wild flower growing around its native Mediterranean. The flowers when they finally appeared were the only part of the plant that looked like the pictures of Alkanna tinctoria seen all over the internet but the roots? The roots were white!

Doing some reading around this ancient dye plant I find that its qualities as a medicinal plant derive solely from the coloured substances in the root which were used as a dye, cosmetic and bio stain so you can imagine the way I feel after lavishing attention on this plant for the last three years only to find the roots are white! Recently I discovered one internet comment on the plant that says the cultivated version of the plant does not produce as much dye as the wild type. Well that’s some understatement. Of course it is possible that lavishing attention on the plant was entirely the wrong thing to do and I should have left it alone but it seems more likely that the growers have simply selected the seed year after year from the largest prettiest plants and in so doing have bred out the qualities that gave the plant its historical value.

Just to confuse matters Alkanna tinctoria has been and is also known as “Anchusa bracteolata, Alkanna tuberculata, Alkanna lehmanii, Lithospermum lehmanii”, and has been given various common names as follows Alkanna Radix, Buglosse des Teinturiers, Dyer’s Bugloss, Henna, Orcanète, Orcanette, Orcanette des Teinturiers, Orchanet, Radix Anchusae. Rühlemann’s who sell the seed are now calling it Alkanna tuberculata. There is certainly confusion on the identity of all these plants. Are they all the same or not. If there are any botanists out there  who can get to the bottom of this please please get in touch!

References

Philip John and Luciana Gabriella Angelini – Indigo – Agricultural Aspects. Chapter 7 of Handbook of Natural Colorants  Edited by Thomas Bechtold and Rita Mussak. Wiley Series in Renewable Resourses. (Available as free download).

Rühlemann’s  This German herb plant and seed supplier has a number of dye plants for sale including Chinese Woad and Long Leaf Japanese Indigo but it is primarily interested in the medical properties of the plants it sells and I get the impression they know little about plant dyeing.

The Natures Rainbow Year – (and its only half way through!)

An article by Susan Dye and Ashley Walker
© copyright 2018

2018 is turning out to be our most successful yet.

The year began with our good friend Brian Bond joining us to deliver a two day workshop in Ipswich in late January with the International Felters Association (see above). Susan was involved in much mordanting in preparation. This was our second major plant dye workshop away from home, and dependent on friends or family to help us with transport. Hard work packing an ‘all singing all dancing’ workshop and the three of us into a single hatchback vehicle (albeit a large one, thanks Brian!). Quite stressful but very well worthwhile, as the students were terrifically motivated and created a full palette of wonderful colour on the finest merino tops.

Also in January we had confirmation that Southwark Cathedral had invited the London Guild of Weavers, Spinners and Dyers (WS&D) to demonstrate plant dyeing as part of London Craft Week in Mid-May. Susan was asked to coordinate the project, having held a successful mini natural dye demonstration there as part of the biennial London Guild exhibition last November.

Preparations for all this activity took place mostly in the winter and early spring when the weather was too cold or wet to work outside on the dye garden

In between scoping and planning the London Guild event at Southwark, Susan gave talks on plant dyeing to the Chelmsford Embroidery Guild, on the red dye from madder for the Cambridge Guild of Weavers, Spinners and Dyers and, closer to home, a talk on the horticulture of dye plants for the Wymondley Gardeners Group. Had the snow in early March not intervened there would have been another talk on the history of Norwich Dyers to region 7 of the Quilters Guild.

London Craft Week event at Southwark Cathedral with the London Weavers, Spinners and Dyers Guild

The Shard overshadows our colour splash at Southwark Cathedral

Susan spent much of April mordanting and test dyeing fabric and yarn for the London Craft Week event, which was to be held outdoors in the Churchyard in mid-May. Fortunately the weather improved and we were blessed with two sunny breezy days. With help from textiles graduate Hannah Sabberton, Susan and I carried Hitchin grown fresh woad and dry Weld, Indigo dye solution, mordanted fabric yarn and fleece, samples, display materials and goodness knows what else (kitchen sink comes to mind!) on the train and bus into Central London at rush hour. We are resourceful public transport travellers with trolleys and backpacks and all arrived safely! Mercifully all the pans and heaters had been supplied by London Guild members based not too far away (thanks to Penny and Diane). Also there were many, many lovely dyers from the Guild who shared the demonstrating. All told there were twenty two volunteers across the two days. We spoke to people from all over the world, from London and other parts of the UK. Tiring but very satisfying to see the rainbow of colours we achieved with just the three medieval ‘grant teint’ plant dyes: Madder, Weld and Woad.

Susan managed to escape a couple of times down to the British Library where she loves to do research on the history of dyeing and in particular the 19th Century “Norwich Red”. An article to be published in the Autumn issue of “The Journal of Weavers, Spinners and Dyers” will detail her findings so far. We have also been asked to write an article on growing dye plants with a particular emphasis on small gardens and container growing. This should appear in the next issue of “British Fibre Arts” along with a profile about ourselves. The Editor Rainy Williamson made us think about what we do and why we do it. I was particularly reminded that many people do not have access to a garden or allotment and may only be able to grow dye plants in small spaces. I immediately set about making and planting up some large-ish containers with suitable dye plants to see how they responded. And then we got to thinking that apart from a couple of small demonstrations and the regular workshops for our local guild we’ve never made an effort to share our skills in plant dyeing with the local population. So Susan quickly got on the phone and asked the Hitchin Festival organisers if they still had some slots left in their programme and lo and behold, (thank you Keith)  we were found a slot in the programme.

Indigo Blue, Weld and Chamomile yellow and Greens produced by overdying yellow with blue and blue over yellow

Results from the green overdye experiment done at the Herts Guild of Spinners Weavers and Dyers Workshop

Meanwhile we had another workshop for our local Guild in North Herts to get ready for. This was based around an experiment investigating the notion that a better green is obtained if wool is dyed first with indigo and then weld (yellow) rather than the other way round as we have traditionally done it. Various accomplished plant dyers had reported this finding and we wanted to check it out. The workshop produced some fantastic greens and, somewhat to our surprise, the blue overdyed with yellow did indeed produce the best green.

While all this has been going on I’ve been working hard on the Natures Rainbow dye garden, getting it into shape to satisfy the North Herts District Council allotment inspector (Grounds Maintenance Monitoring Officer). Because we are growing a most unusual set of crops some of which look remarkably like weeds we

Rubia tinctorum

Madder is closely related to the weed Cleavers or Goosegrass. It looks and behaves much the same but is altogether larger in stalk and leaf and has berries instead of hard seeds.

Ransoms Rec Allotments, Hitchin

The Natures Rainbow allotment plot in early June.

have to make the plot look as tidy as possible. Madder for example is a close relative of the weed Cleavers and has the same sprawling habit and Weld is generally classified as a weed anyway. In addition, we leave our second year Woad plants to go to seed, so we have stock for the following year and this too raises eyebrows.

Asperula tinctoria

Dyers Woodruff in flower

We also decided early on this year that if we are going to continue giving talks and writing articles about growing dye plants then we need to expand our experience and grow some of the more unusual dye plants so we sent off for more seeds including Chinese Woad, Wild Madder, Field Madder, Ladies Bedstraw, Blood Root and where we couldn’t get seeds we ordered plants. These include Dyers Woodruff, Black Oak, and Smooth Sumac (Rhus glabra).

Quercus velutina

Our new Black or Quercitron Oak Sapling. The inner bark of this North American tree produces the dye quercitrin which for a while was a major industrial source of yellow dye. Of course it will be many years before we can harvest any bark from this specimen!).

Reseda luteola

Honey bees are particularly fond of Weld

 

 

 

 

 

 

 

 

As a beekeeper I’m also very interested in growing plants that are also good for all kinds of bees so I’ve been very gratified that many of our dye plants are also fantastic bee plants too, Weld and Japanese indigo are two of the best.

Rhus Glabra

Smooth Sumac from North America, the dried leaves of which contain 25-27% by weight of tannins.

Look out for more blogs detailing some of the events mentioned here but you might have to wait until things calm down a bit before we get time to write them!

Inula helenium

Elecampane – Inula helenium

An article by Ashley Walker
© copyright 2018

When we first became interested in growing and using dye plants we came across an entry in “Traditional Scottish Dyes and how to make them” by Jean Fraser. This seemed to us to be very exciting because it offered a tantalising alternative blue dye to Woad indigo.

Traditional Scottish Dyes and how to make them by Jean Fraser

Page 69 from Jean Frasers book – Traditional Scottish Dyes and how to make them.

Traditional Scottish dyes and how to make them by Jean FraserWe immediately set about obtaining some seeds which were readily available as Elecampane is a popular garden flower and ancient medicinal herb. Our first lot of seedlings were all eaten by slugs but the second batch (protected until they were larger) survived to produce two small beds.

It took a number of years for the plants to reach full size but by this time we had realised that the likelihood of obtaining blue from the roots was very unlikely and we had discovered Japanese Indigo so did not think it worth even trying. We kept the plants because every year we are rewarded with a sunny display of glorious yellow flowers which act as magnets for bees of all kinds. These tall plants with giant leaves are low maintenance and just take care of themselves.

Inula helenium

Honey bee on Elecampane flower.

The Dye garden has grown over the years and we are getting to the point that every plant species we grow has to justify its presence by being a proven source of plant dye. But still, the mystery of Jean Fraser’s entry stuck in our minds so this year I decided to give it a go before the plants started to grow.

Three of the incomplete “no details or quantities given” recipes mention whortleberries and one recipe Elder (presumably berries) as additives to improve the colour. We know by now that most black berries can give pinks, lilacs and mauves with a good alum mordant but they are not lightfast, iron mordants are best at prolonging the life of fugitive dyes and the fourth recipe mentions iron so we thought it worth obtaining some whortleberries . What are whortleberries?

Wikipedia suggests they are one of three possible members of the Vaccinium family:

Vaccinium myrtillus, bilberry, or blue whortleberry
Vaccinium vitis-idaea, lingonberry or red whortleberry
Vaccinium uliginosum, bog whortleberry/bilberry

All three plants grow commonly in Scotland but we think it is a reasonable guess that the name refers to the bilberry V. myrtillis or uliginosum as vitis-idaea is a red berry. The closest source of berries we could get hold of were supermarket blueberries (probably Vaccinium corymbosum). Not as good as our native bilberries as they only have a blue black skin and internal pale green flesh. Our native species are blue/black throughout.

Experiments

Initially we tried a number of variations:

  1. Fresh chopped and bruised roots heated with and without blueberries
  2. Fermented chopped and bruised roots with and without blueberries
  3. Samples of unmordanted, alum mordanted and iron mordanted wool were added to each of the dye pots (the root and berry material were not removed).

The roots of elecampane are white with a yellowish skin and black bark which is not attached to the root and is easily washed off. There appears to be no colour in the root at all!

Inula helenium

Elecampane root

Inula helenium

Elecampane cut root

Because of this lack of colour we had long suspected that the only possible source of colour would be from tannins in the root reacting with the iron mordant to give a grey. We suspected that in Scotland grey was often called blue and with the addition of some whortleberries a bluish grey could be obtained though it would fade to grey over time. As there are many other sources of tannin in the dye plant world we were sceptical that Elecampane root would give us anything worth having.

Results

The results were fairly conclusive in that the only significant colour change occurred with the iron mordanted wool where a silvery grey was obtained from the fresh root and a yellowish grey from the fermented root. The unmordanted wool stayed white and the alum mordanted wool turned a very pale yellow. The addition of blueberries made little difference.

Inula Helenium dyed wool

Right: iron mordanted wool in fresh root dye bath. Left: Iron mordanted wool in fermented root dye bath.

Inula helenium treated woth iron mordant

On the left cut root treated with iron mordant. On the right untreated root.

Painting an iron mordant solution onto cut plant material usually shows up the presence of tannins fairly rapidly but sometimes it takes a few hours to get a colour change. The elecampane root had to be left overnight before the change seen here on the left took place. Other additives mentioned in the recipes are salt and ash. Dipping a cut root in salt had no effect but adding a tiny amount of sodium hydroxide (an alkali in wood ash [lye]) to the cut root turned it immediately yellow and after 24 hours a yellowish dark grey. We did not use any of this alkali in our experiments as we were particularly interested in obtaining a neutral or blue grey but it looks like adding the alkali could aid in getting a darker colour.

Once we were happy we could get this neutral grey we went ahead with dyeing a large skein of hand spun yarn (about 100g) mordanted with 1g of ferrous sulphate*. This was added to a dye bath made from about half a kilo of chopped and bruised Elecampane root heated to around 90°C and left for one hour then strained to remove the solids.

Inula helenium dyed wool

100g skein of hand spun iron mordanted wool dyed with Elecampane root.

OK, so no blue, but a good neutral grey is hard to obtain as most tannin rich plants have additional dye stuffs and the greys obtained are tinted with yellows or browns. Elecampane is almost free of any of these contaminants. As any designer will verify grey has the ability of amplifying adjoining colours making them seem brighter than they really are. A dye garden without a source of grey would not be complete so the Elecampane stays!

Inula helenium

Elecampane in full flower

*The iron mordanting is done according to Liles method using the same quantity of oxalic acid as ferrous sulphate. The Oxalic acid prevents the iron from oxidising from the yellow-green ferrous sulphate to orange ferric oxide (rust).

References

“Traditional Scottish Dyes and how to Make them” by Jean Fraser. Illustrated by Florence Knowles. © 1983, 85 and 96.

“The Art and Craft of Natural Dyeing – Traditional Recipes for Modern Use” by J. N. Liles. © 1990

Colour in Winter 2018

In January two years ago I ran a plant dye workshop for Region 5 of the International Feltmakers  Association. One thing leads to another and … by way of the IFA AGM last Spring, I was invited to run a similar workshop this January for the Region 7. And what a delight it was!
Thank you to Sally Sparrow for organising the event.

With my friend Brian’s most excellent vehicle (I don’t run a car), and not a little anxiety as to whether I had packed everything we needed, we installed my dye studio in a scout hall in the outskirts of Ipswich for the weekend.

Dye woerkshop2-small

The venue was large and well appointed with power sockets for my preferred heat sources – portable electric induction heaters (you can see them in the background in the picture above).

By the end of the weekend nine enthusiastic participants had applied a good palette of natural colour onto nearly 2kg of pre-mordanted fine wool and silk. If you would like to know more and see some great photos, check out Kim’s blog at flextiles here and here. Kudos to Kim, for the excellent write up!

We used home grown madder for pinks and reds, home grown weld for acid yellow and for blue we used bought in woad powder and natural indigo (because at this  time of year you can’t use fresh leaf). We also added in some oranges from dyer’s coreopsis and warm yellows from dyer’s chamomile, both from stock of our home grown, dried flowers.

Here are just some of the colours we obtained.

blog post washing line

 

Chamomile on silk-small

 

 

Madder recipe A on Woo-smalll

 

 

 

 

 

 

 

My aim was for people to get lots of hands on experience working with the dyebaths, to be free to spend most time on the colours that most interested them and get some theory and tips on good practice. I also like to make sure everyone goes home with enough fibre to use in a project. And finally, because I can’t resist the technical detail, there are handouts to read later.

blog post image drying rack

The workshop couldn’t have run without my two helpers. My partner Ashley ran the indigo vats at one end of the room while I set up madder and weld dye pots at the other. Brian Bond, a longstanding friend and collaborator, was invaluable as all round helper.

For inspiration, Brian brought along his glorious plant dyed and hand spun yarn and knitted garments to display. Ashley brought his current work in progress – darned squares of which he needs to make 144 to complete a blanket.  And I set out my collection of fabric and thread samples.

This kind of workshop has long been a regular feature of my local Spinners Dyers and Weavers Guild.  We usually hold these events outdoors on a long summer’s day which works really well for rinsing and drying. I’m looking forward to running the next plant dyeing day for the North Herts Guild of Spinners Dyers and Weavers on Saturday 26 May 2018.

Contact me if you are interested in hosting a plant dyeing workshop. I am open to designing events to suit specialist audiences.

Note on blue: We were using a combination of commercially produced woad powder and natural indigo. To save time at the workshop, these were made up into separate pre-reduced stock solutions.  We discovered that the woad powder was considerably less concentrated  than the natural indigo. As a result the woad stock solution was over-reduced. The natural indigo produced some very dark blues (see below). Whereas the woad vat was over-reduced and it wasn’t possible to apply a deep colour, no matter how many dips we did. We plan to do a controlled experiment comparing the strength of different commercially available woad powders – so check back for more details.

small dark indigo drying

Persicaria tinctoria

Three strains of Japanese Indigo tested and observations on indigo extraction

An article by Ashley Walker
© copyright 2017

This year I had planned to carry out a tightly controlled experiment to look for variation in the amount of indigo produced by three fairly distinct strains of Japanese indigo. However due to a prolonged and still undiagnosed illness, my plans were thwarted and the experiment did not work out quite as I had hoped. However, on 12th and 13th October 2017, with help from Brian Bond another keen plant dyer, I did manage to complete a test of the three plants although the results are not directly comparable due to different planting times and maturity of each variety.

The strains

Broad or Rounded leaf indigo

Persicaria tinctoria

Round or wide leaved Indigo. Directly sown bed

Grown from seed originally from the USA (from fellow natural dyer Pallas Hubler in Washington State on the west coast) who sent a few seeds over to Brian in 2013. We have been growing and saving seed from this strain ever since so it is possible that it has become adapted to growing in our soil.

  • Late flowering (October into November)
  • Pink Flowers
  • Compact short flower stems
  • Wide short or rounded leaves
  • Foliage pale to mid green
  • Easily damaged by high nitrogen levels in the soil. Grows poorly in cool overcast weather.

Long leaf indigo

Persicaria tinctoria

Long leafed Japanese Indigo in full flower.

Seed for this was obtained from the German supplier Rühlemann’s. Unfortunately this was in full flower by the time I was able to harvest it for the test and from previous experiments I know that once indigo has committed itself to flower production the amount of indigo in the leaf falls dramatically.

  • Large long pointed leaves
  • Pink flowers
  • Long delicate flower stalks
  • Early flower (September-October)
  • Dark green leaves
  • Very tolerant of high nitrogen in the soil and generally more robust.

An in-between white flowered strain

Persicaria tinctoria

Intermediate white flowered Japanese Indigo

Persicaria tinctoria

Intermediate strain of Japanese Indigo with white flower.

The seed was obtained from Lisa George Fukuda a fellow plant dyer in Guernsey who had it originally from Teresinha Roberts at Wild Colours

Unfortunately this was planted out late in the year (August) so as yet I know little about its habit as there has not been enough time for it to grow to full maturity.

  • Longish leaves
  • White flower
  • Easily damaged by high nitrogen fertilizer.
  • Mid green leaves
  • Quickly bushes out, highly branching.

All three strains were grown on the Natures Rainbow allotment in Hitchin in a chalk soil with a strong application of Fish, Blood and Bone plus some chicken manure pellets.

Persicaria tinctoria

Leaves from all three strains.

Persecaria tinctoria

Rounded leaf Japanese Indigo growing with the Long Leaf strain in the greenhouse. Here they look like two completely different species.

The experiment

After stripping the leaves from the freshly cut indigo stalks, 220g of leaves from each strain were slowly heated from room temperature to 80°C in stainless steel pans with 4 litres of tap water. The pans were stirred at short intervals throughout. Note: the weight of leaves was determined by the amount of the long leaved strain that I could harvest from shoots that had not yet come into full flower as I wished to minimise the effect of flowering on indigo production. The amount of water in the pans was deliberately large as I wished the final colour to be on the pale side as variations in pale colours are easier to distinguish. More water also means the pot is easier to stir before the leaves are cooked.

Heating to 80°C took about 35 minutes. The pans were then taken off the heat and allowed to cool, free standing in the air for 1 hour. (The air temperature was appoximately 20°C).

Persicaria tinctoria

Intermediate Japanese Indigo extraction bath with container of liquor to show gray colour. Photo taken just after pan was removed from the heat.

At this point no difference could be noticed between the different pans. The liquor in each pan being a pale greyish blue in each case.

After one hour the leaves were removed by straining through an old pair of tights into a large plastic bucket. Half a cup of household ammonia was then added to the liquor. Taking care not to breathe in hot fumes, this liquor was poured back and forth from bucket to pan 10 to 15 times to aerate and oxidise the indigo precursor to indigo. The colour of the liquor changed from grey to yellow green, with the round leaved plant giving the darkest colour change and the long leaved plant the least. This is a good indicator of how much indigo is present in each pan.

Once oxidised to indigo, the liquor is now in a stable form and can be left for long periods without any loss of indigo. The reduction vats (indigo dye baths) were set up the following day as follows. The pans were heated to 50°C, one level teaspoon of Spectralite (Thiourea Dioxide) was added to each pan, gently stirred in and left for 30 minutes for the indigo to reduce to its soluble form. Identical weight skeins (26g) of wool were added to the baths at 50°C and left for 20 minutes before removal and oxidation in the air. The dye baths were kept in a hay box to maintain constant temperature during the dyeing.

The results

Japanese Indigo

First results showing a surprising difference in colour obtained

The long-leaved plants (left) were disappointing only producing an ice blue colour. The white-flowered intermediate-leaved plant gave a slightly deeper shade but still pale (centre). The round-leaved plant produced a respectable light blue (right).

The poor results for the long-leaved plants was understandable because of their flowering state, however I was surprised the colour was quite so pale. The good results for the round-leaved plant was a real surprise as I had become convinced these plants would not be the best. Overall the pale colours made me worry that I had not optimized the process and I decided to repeat the experiment for the round-leaved and intermediate-leaved white-flowered plants (I had no more of the long-leaved plant so I could not replicate this one).

On the second run I made one change which was to slow the cooling of the extraction bath after reaching 80°C by placing the pans in hay boxes. For this experiment, using 4 liters of water I was aware that this small amount of liquor would cool quickly, perhaps too quickly? An experiment we conducted some years ago revealed that premature cooling of the extraction bath resulted in a dramatic loss of indigo when processing woad leaves. Two years ago we discovered that leaving the bath at a high temperature for more than one hour also results in a loss of indigo so I have become wary of putting large baths in hay boxes which are capable of maintaining a high temperature for hours.

In this second run the results from the white-flowered intermediate-leaved plant improved but the round-leaved plant still produced the better result (which itself was no better than in the first run).

Skeins of wool dyed with Japanese Indigo

Second run with intermediate white flowered indigo plant compared to rounded leaf plant.

Skeins of wool dyed with Japanese Indigo

Comparison of intermediate white flower strains. The difference between quick and slow cooling of the extraction bath.

Wool dyed with Persicaria tinctoria

No real difference between runs for the Rounded leaf strain.

Discussion

In theory all three plants should have produced broadly similar amounts of indigo. That they did not could have been due to genetic differences but as noted above all three plants were at different stages of development having been planted at different times and the round-leaved strain had possibly adapted to the local soil over the 4/5 or so years I have been growing it. The poor results from the long-leaved plant may have been entirely due to their flowering state. The intermediate-leaved white-flowered strain had only been planted out in late August and may not have had sufficient exposure to the sun to develop much indigo.

The diversity of results shows how critical it is to grow and harvest the plant at the right time. I was certainly concerned that harvesting the plants in October was a risk, as all three varieties were producing flower buds (although only the long-leaved plants were in full flower). Later I extracted a concentrated bath of indigo by making up a large pan crammed full of leaves and only enough water to barely cover the leaves when they were pressed down forcibly. The results were pleasingly strong indicating that the leaves were still fully charged with indigo.

Skein on right dyed with a strong indigo dye bath

Skein on right dyed with a strong indigo dye bath

I will certainly be making strenuous efforts to continue to save the seed from the round leaf strain whatever the reasons for the underperformance of the other two strains!

Confirmation of results

Since this post Leena Riihelä writing in her blog (see Riihivilla) has confirmed that the long or pointed leaf variety of Japanese Indigo does not produce as much indigo as the broad or rounded leaf variety. Leena who also grew three strains of Japanese indigo this year also speculates that the broad leaf (rounded) variety originated in Japan. (The long leaf variety may come from Northern Japan or China). She is also able to confirm that the long leaf variety flowers much earlier. Leena is based in Finland which has such a short growing season that the rounded leaf variety does not have time to produce seed. Leena has a wealth of experience to share about indigo and other natural dyes so please visit her blog and web site. (see below)

Thanks to:

Brian Bond
Leena Riihelä at Riihivilla
Lisa George Fukuda
Pallas Hubler

Indigo dyed wool

The range of blues obtained from the three strains of Japanese indigo.