Category Archives: growing dye plants

This is for posts that describe how to grow dye plants

Shows Devil's Bit Scabious plant in early June with lush green leaves but not yet in flower. Inset is blue composite flower from previous year

Devil’s Bit Scabious as a source of indigo?

By Ashley Walker
Copyright 15th June 2019

Scan of page 62 of Traditional Scottish Dyes by Jean Fraser showing entry on Devil's Bit Scabious

Scan of page 62 of Traditional Scottish Dyes by Jean Fraser showing entry on Devil’s Bit Scabious.

Front cover illustration showing plant dyed yarns

Scan of original reference from Chemical Dictionary of Economic Plants aparently confirming that a blue dye can be obtained from this plant

Reference to Devil’s Bit Scabious from Chemical Dictionary of Economic Plants

Some years ago I came upon a reference to this bee-friendly and pretty blue flower being a potential source of blue dye in Jean Fraser’s book “Traditional Scottish Dyes and how to make them”. Jean attributed her information source to Ethel Mairet. In her 1916 “Book on Vegetable dyes” Ethel briefly mentioned that Devil’s Bit Scabious leaves, if treated like Woad, will give a blue colour but adds no further details. A quick internet search brought up a number of other references to this plant producing either a blue or green dye. Significantly an entry in “Chemical Dictionary of Economic Plants” (2001) edited by Jeffrey B. Harborne, and Herbert Baxter, states that fibres placed in an alkaline fermentation bath of the leaves will turn blue on exposure with the air, though the active chemical is not identified as indigo. Devil’s Bit Scabious (Succisa pratensis) a member of the honeysuckle family (Caprifoliaceae) and a related plant is Teasel (Dipsacus), which in turn is also mentioned as a source of blue dye – being apparently produced by dried flower heads.

At the time I was looking out for possible dye plants that had flowers that weren’t yellow, as this would make our dye garden a little more attractive to the eye. I am also a beekeeper and Devil’s Bit Scabious was being promoted as one of the most pollinator-friendly native flowers, so I set about obtaining some seed. I was disappointed however to find that although you can buy the seed it has very poor viability. My first attempt resulted in no germinations and the second attempt only produced 5 plants out of around 500 seeds. In the end I bought some plants from the Rosy Bee plant nursery and planted them in the dye garden where they have positively thrived. Finally (3 years later) I had enough plant material to try extracting the blue dye.

Method

Leaves of the Devil's Bit Scabious looking very much like Woad leaves

Basal leaves of Devil’s Bit Scabious which bear close resemblance in both size, colour and shape to Woad leaves.

All references to the extraction process say that the basal leaves should be used and that they should be treated just like Woad i.e. placed in an alkaline fermentation bath (possibly the urine bath). I was not happy about using urine, so instead opted for Jenny Dean’s recipe for hot extraction of indigo from Woad using ammonia as the alkali. In addition, I did a more conventional dye extraction by simmering the leaves for 1 hour and straining the liquor; then dyeing mordanted wool yarn in a heated dyebath with and without adding soda ash to raise the pH. Finally I set up a solar dyeing jar with leaves, wool yarn and some soda ash to make the liquid alkaline and set it aside in a warm place to ferment.

Results

Jenny Dean’s indigo from Woad extraction

After pouring boiling water over the leaves and leaving for an hour and straining, I obtained a pale yellow liquid.

Shows pale yellow colour of Devil's Bit Scabious liquid extract

Pale yellow liquid extract.

showing green liquid produced by adding ammonia

Adding the ammonia turned liquid a dark green.

 

 

 

 

 

 

shows colour change from dark green to orangy yellow after reducing agent added

Colour change after adding Thiourea Dioxide to the green liquid.

There was no sign of any free indigo nor the characteristic sherry colour from Woad. The next stage, adding the alkali and aerating was exciting because the liquid quickly went a lovely dark green, exactly as one might expect if there was indigo in there. I had my hopes up now for the first time! The next stage was to add a reducing agent and for speed I used a tiny amount of Thiox (Thiourea Dioxide). The colour of the liquid immediately changed to an orangey yellow – too fast for the normal indigo process.

Both samples of yarn shown are the same shade of white

Unmordanted raw wool yarn vs unmordanted dipped yarn. Left: raw wool; Right: dipped wool.

But I put in some un-mordanted wool yarn anyway and waited. I took the yarn out but obtained no discernible change in colour at all. Disappointment! I did several dips and left the yarn in for about 15 minutes, then did more dips, but sadly there was no colour change.

After drying, the wool does look slightly altered but it’s a bit of a stretch of the imagination to see any blue.

Later, I took some of the original green coloured liquid which had the alkali added and neutralized it with some distilled vinegar. The colour instantly changed back to yellow, indicating pretty conclusively that there was no indigo in it.

Color changes from green to orangy yellow when liquid is neutralised with white vinegar

lowering the pH of the green liquid with vinegar brings it back to an orange yellow.

Conventional extraction

Pale yellow alum mordanted wool top. Grey iron mordanted wool bottom

Mordanted wool yarn dyed in liquid extract before alkali was added.

Alum mordanted wool gave a pale straw yellow with no hint of green. Dyeing time ½hour.
Iron mordanted wool, unexpectedly, gave a rather nice slightly warm grey. Dyeing time 15mins.

Shows different colours obtained by mordanting the wool with alum, copper and iron

Colours obtained with three different mordants after leaving in alkaline Devil’s Bit Scabious dye bath over night.

After adding the soda ash, the liquid darkened off as expected to a greeny yellow though not as green as when using ammonia. Wool samples mordanted with alum, iron and copper were introduced and, after rinsing in clean water, produced a similar set of colours after about ½ an hour. At this point I decided to leave the samples in overnight. In the morning the alum mordanted sample was much the same but the iron mordanted sample had turned from grey to a warm brown. The copper mordanted wool was an attractive greenish bronze. Depth of colour had not increased during the night. Rinsing the yarn removed the green tint of the dye bath.

Discussion

The acute sensitivity to pH tells me that the chemicals producing the green colour in the alkali extract are not dyes and will not even attach to mordanted wool. The grey and light brown colours obtained with mordanted wool suggests that there are natural tannins in the leaves and also a yellow dye. The entry in the “Chemical Dictionary of Economic Plants” says the active dye chemical is a seco-iridoid glucoside. Internet searches suggest that these molecules protect the plant from predators and pathogens and are of interest for their anti-oxidant, anti-inflammatory and possible anti-cancer properties. I did find a reference to an iridoid called genipin which in a weak acid is reported to produce a soluble blue pigment in the presence of oxygen with potential as a food colourant. But to obtain this blue pigment seems to require a chemical laboratory! And there appears to be no logical chemical link to the indigo molecule.

I speculate that the mythical blue colour is one of those confusions that get passed from one source to another without anyone really testing it out. If by some miracle there is a blue dye to be had it is not indigo. Possibly someone at some point mistakenly put Woad leaves into a bath of Devil’s Bit Scabious, they are remarkably similar in shape and size. Or perhaps someone just assumed that since the blue/green was obtained in an alkaline bath identical to a Woad leaf extraction bath then they must be the same dyes.

Shows jar filled with leaves of Devil's Bit Scabious, water with a bit of soda ash added and wool yarn.

Hopefully this solar dye jar experiment is about as close as I can get to the original assertion that Devil’s Bit Scabious fermented in an alkaline liquid will give blue.

The results of the solar dye experiment will take some time. I think it is unlikely there will be any blue or green but we will see.

One further thought, there could be a bit of a pattern developing here, searching for a blue from Elecampane root (see blog post) I discovered a rather nice grey could be obtained. Here again I get another grey. Perhaps this is more evidence that the colour grey was often referred to as blue in earlier days.

Well, I’m keeping the Devil’s Bit Scabious in the Dye garden. It really is a fantastic pollinator-friendly plant and it looks good too.

References

Handbook on Natural Pigments in Food and Beverages – Industrial Applications for Improving Food Color. Edited by: Reinhold Carle and Ralf M. Schweiggert. 2016.

Jenny Dean’s Wild Colour. http://www.jennydean.co.uk/

Resources

Rosy Bee – Plants for bees.
http://www.rosybee.com/plants/devils-bit-scabious-succisa-pratensis

Image showing young seedlings of Japanese Indigo in premature flower

Premature Flowering in Japanese Indigo

By Ashley Walker
Copyright 10th June 2019

This year I’ve had two reports of people in the UK growing Japanese Indigo from our seeds and experiencing premature flowering in May. I also read with interest Deb McClintock’s blog post about her early self-seeded Japanese Indigo (in mid-Texas in the USA) which germinated in early February and flowered in May. In the first two cases the plants were not remotely big enough to harvest, so this is very disappointing – doubly so since once the plants put out flower heads the amount of indigo in the leaves starts to decrease. Deb McClintock was able to harvest her “bonus crop” but she noted that it had not grown as well as her normal summer crop. Ideally the plants should grow to a large size before flowering in August/September.

So what is going on and what can be done to prevent this?

In all plants, flowering is often stimulated by the experience of stress e.g. unnaturally high or low temperatures, insufficient water or nutrients and pest damage. However, in the above examples the plants were being treated very well. My first thought was that the main cause of the early flowering was day length. In all three cases the Japanese Indigo seeds germinated in January/February when the day length is short. However, I can’t rule out low temperatures since this is the middle of winter in the UK (latitude=50deg N) and the night-time temperature in Mid Texas is going to get pretty low. Also in the UK in 2019 we experienced a Spring with extreme temperature swings and unusually late frosts.

I can find no definitive information online to suggest that low temperature is a known trigger for flowering in Japanese Indigo. But looking in my copy of ‘Handbook of Natural Colorants’ I see that day length is reported as the critical factor for Japanese Indigo, but other influences are not excluded. However it does say that Chinese Woad (Isatis indigotica) will flower if it experiences night time temperatures below 10°C (50°F).

In all three reports of early flowering, the plants received no artificial lighting and were grown in relatively frost free conditions, although they probably did experience night time temperatures well below 10°C. But of course the day length conditions in mid-Texas are considerably less variable than in the UK. (Mid-Texas latitude is approx. 35 degrees North compared to approx. 50 Degrees North here in Southern England).

The Handbook of Natural Colorants recommends sowing Japanese Indigo in April in mid Europe, with a first harvest in July or early August just before the flower heads start to form. It’s interesting to note that by this point in our summer, the day length has started to shorten but night-time temperatures are usually still over 15°C (60°F), so that should rule out cold temperatures as a trigger and points the finger at shortening day length.

However, my own observations in Hitchin for 2018 is that flowering was very late (September/October) following an exceptionally hot long Summer and warm Autumn. This is a much later flowering than normal.  This is confusing because it suggests that the high temperatures prevent day length from being the dominant factor in triggering flowering. No doubt someone out there (perhaps the professional Japanese Indigo farmers) will know the definitive answer but at the present time I’m not sure if it is short day-length or temperature stress which is the most important trigger for flowering. But in either case the solution is the same.

In Southern England, no matter how warm the early Spring, don’t be tempted to sow your Japanese Indigo seeds before April, unless you are able to give them some artificial light to lengthen their day. Giving them a little warmth (particularly at night) is a good idea too. If the plants do start flowering early, pinching out the whole top of the plant may reset them back to vegetative growth. If the plants are large enough it may also work to take stem cuttings in water (cut out the flowering tips). If these measures fail, new seeds can still be sown as late as June in the South of England.

shows seeds being propagated with extra lighting supplied by a rack of flourescent bulbs. Purpose is to boost light levels to stop seedlings becomming "leggy" and also to increase day length

In my own case, I use heated seed trays and artificial lighting on a timer.

 

Happy growing!

References

Handbook of Natural Colorants (2009), edited by Thomas Bechtold and Rita Mussak, Chapter 7 by Philip John and Luciana Gabriella Angelini.

Deb McClintock’s blog, https://debmcclintock.me/2019/05/27/new-tools-dried-indigo/

Thanks to:

Brian Bond for the photo of Japanese Indigo in premature flower.

Sue Prior

Field Madder plant showing tiny pink four petaled flowers

Natures Rainbow Garden Update – Spring 2019

By Ashley Walker
Copyright 8th May 2019

The weather here has followed the pattern of recent springs by being dry, sunny and warm with cold intervals and frosty nights. Planting out of the Japanese indigo will have to wait for a week or two yet but most plants are thriving. Time to look at last year’s plantings and make an assessment of what has worked and what has not. Last year we embarked on growing a number of new plants, many of which are relatives of Common Madder. Of course many folks have said “What on earth are you doing that for? There is no better plant than Common Madder!” That of course is true but in the past many of these madder relatives were used as dye plants and prized for their colours so we thought we’d try and find out for ourselves how easy they are to grow and eventually what colours their roots will yield.

Wild Madder Rubia peregrina

We first started with Wild Madder (Rubia peregrina) three years ago now. Spring frosts have been particularly hard on the plants as their evergreen upper leaves are not particularly frost hardy.

Browned and crisped frost damaged evergreen leaves of Wild madder, Rubia peregrina.

Frost damaged evergreen leaves of Wild Madder.

Their native UK homelands are the southern coastline of Devon, Cornwall and Wales where they get warm sea breezes that usually prevent frosts, so here in Hertfordshire they are a bit out of their depth. However the roots are protected and soon shoot back once the warm weather returns. Getting a good harvest from the plant is going to take time, even without frosts it’s very slow growing so we’re not planning to dig any up until Autumn this year.

Shoot of Common Madder (Rubia tinctorum) showing browned shoot as a result of frost damage.

For the first time in many years our Common Madder shoots were badly frosted. Not a problem as the plants quickly produce new shoots

Even our Common Madder beds were badly affected by the frosts with many of the new shoots being crisped.

Field Madder Sherardia arvensis & Hedge Bedstraw Galium mollugo

Field Madder Sherardia arvensis A cushion of Field Madder growing under a Weld plant with Sawort to the left. This plant self seeded last year and has come through the winter without any frost or snow damage.

A cushion of Field Madder growing under a Weld plant with Sawort to the left. This plant self seeded last year and has come through the winter without any frost or snow damage.

Generally described as an annual weed, we discovered that given plenty of attention this plant is perfectly capable of going through the winter and withstanding any frosts. Does this make it a short lived perennial? Many hardy annuals can do this and provided they are watered and fed can keep on growing. As this plant has very thin roots, getting a harvest is obviously going to be a bit of a test so we’ve decided to do a little experiment by growing Field Madder and another similar relative Hedge Bedstraw Galium mollugo in large pots in a compost mix that should be easy to wash away from the roots at the end of the year.

Large plant pot containing seedlings of Field Madder Sherardia arvensis

Large pot with seedlings of Field Madder.

Hedge Bedstraw Galium mollugo

Large pot of Hedge Bedstraw seedlings.

Dyer’s Woodruff Asperula tinctoria

Over the winter I managed to get hold of some seeds from Rühlemann’s in Germany but unfortunately none of these have thus far germinated. As a native of the northern steppe lands of Europe and Asia this may mean they need vernalization. Some of the plants we obtained from Scottish plant nursery (Poyntzfield Herb Nursery)  died towards the end of last year. Plants placed in an ericaceous compost in tubs seemed to do better than those planted in the chalky soil of our Nature’s Rainbow dye garden. This goes against the generally accepted advice that the plant likes alkaline soils. However, It may be other factors were involved. All of our plants died back really quite early in the year and we were afraid they might die out altogether, but back they have come this Spring and they look quite healthy. They have reappeared at the edge of the planters, showing that last year they tried to expand by producing underground stems much like Common Madder. I guess that this means they are capable of also being quite invasive!

Feathery Green shoots of Dyers Woodruff Asperula tinctoria

New shoots of Dyer’s Woodruff in the alkaline soil of our dye garden.

Ladies Bedstraw Galium verum

This plant has done really well in a whole variety of settings and soil types. It’s also very well behaved with minimal spread. It looks good throughout the year, with pretty clumps of feathery foliage followed by a spray of small yellow flowers in the summer. With its historic interest as a bedding straw, its use in dyeing  and its versatility as an ornamental garden plant, I feel that this plant is a must for any dye garden.

Feathery green clumps of Ladies Bedstraw Galium verum growing next to the greenhouse.

Clumps of feathery green Ladies Bedstraw growing by the greenhouse.

Alder Buckthorn Rhamnus frangula & Purging Buckthorn Rhamnus cathartica

Alder Buckthorn Rhamnus frangula. New shoot showing "alder " shaped leaves and blossom buds.

New growth of Alder Buckthorn.

New growth of Purging Buckthorn Rhamnus cathartica

New growth of Purging Buckthorn.

We tried planting Alder Buckthorn, an acid soil loving shrub, in a variety of conditions. Those planted in ericaceous beds or tubs have done well but those planted out in a wild setting in the chalk soil here have suffered greatly, though it has to be said, the most damage was done by muntjac deer who clearly have a liking for it.
The Purging Buckthorn did less well, to my surprise. It’s not supposed to be fussy about soil type. No casualties, but the plants have not grown very much in the last year. Although it could be that this plant simply takes longer to get established. The new growth this year looks a lot better.

As yet the plants are too small to risk any harvesting but I suspect it is the Alder Buckthorn that will give the better dye.

Tibetan Madder Rubia Cordifolia (Indian Madder or Munjeet)

We are now the proud owners of one of these plants. Obtained from the German Herb nursery Rühlemann’s, this plant spent four and a half days in a box being transported across Europe, the English Channel and finally to our door and arrived in perfect condition! Many thanks to Rühlemann’s  for doing such a professional job of packaging it up, we have great admiration! The growing tips had faded a little during transit but greened up rapidly on exposure to light.
According to the literature these rather elegant looking plants should just be able to survive outside in the UK, though I’m not taking any chances until I’ve had a chance to propagate some cuttings.  At first sight it looks quite different to Common Madder but it has the same leaf whorls (but only 4 leaves to a whorl as opposed to Common Madder’s 4 to 6) and has hooks on the square and weak stems just like madder and cleavers. It obviously has the same growing strategy i.e. it clambers over other plants, holding on with its small hooks.

Tibetan Madder Rubia Cordifolia (Indian Madder or Munjeet)

The Munjeet plant about a week after arriving. Repotted to a larger pot and already starting to grow and looking very healthy indeed

Rubia Cordifolia plant just after delivery and repotting

Rubia Cordifolia plant just after delivery and repotting

We are ridiculously excited by this latest acquisition and look forward to see how it grows and what sort of dye giving roots it has. According to Cardon* its chief dye substance is munjistin which gives a very bright orange. Like common madder it also contains many other dye stuffs, including a very large range of yellow to red anthraquinones. Alizarin is present but only in small amounts so the overall light fastness is probably not as good. Cardon mentions that there are different varieties of cordifolia as well as a very closely related species (Rubia akane) that grows in Japan. Our plant is advertised as being from Tibet, so hopefully it will be able to cope with frost during the winter.

Self-seeding

Bed of hundreds of tiny self seeded Weld seedlings

A mass of tiny self-seeded Weld seedlings in the dye garden

Cota tinctoria

Self-seeded Dyers Chamomile seedlings

 

Madder Seedlings Rubia tinctorum

This year we have had a number of self-seeded Common Madder seedlings in planters positioned near the house. They have produced seedlings in the garden during the Autumn before now, but these usually die during the winter. I think the weather has been just right this year to encourage spring germination and the temperatures near the house have prevented any frost damage.

 

 

 

 

 

Finally a little note on self-seeding of dye plants. We have always tried to encourage plants to self-seed in our garden, with some success. We have been growing the plants for a long period now and the soil is loaded with seed. Weed plants have been under control for several years, so there should be nothing to stop those plants which can self-seed from doing so. So here’s a check list of what you need to do to follow suit:

  1. Allow your plants to flower and drop their seeds. This can produce, in some people’s eyes, an untidy garden but there are so many advantages including encouraging wildlife and saving your time growing the plants from seed and planting out every year.
  2. Keep your garden weed free.
  3. Dig your garden sparingly, preferably in the Autumn or Winter.
  4. Learn to recognise dye plant seedlings.
  5. Use mulch sparingly i.e. only on areas where you intend to plant out other plants. (Mulch supresses seed germination and encourages slugs and snails).
  6. Try and control slugs and snails. (I recommend organically approved slug bait [Iron phosphate] as a last resort).
  7. Water the bare soil if it becomes very dry.

Three varieties of Japanese Indigo Persicara tinctoria

Finally I have managed to sow all three varieties of Japanese indigo at the same time to complete our comparative studies (see blog post). Sure enough, it is possible to tell the difference between the long leaved variety and the broad leaf variety. Even the photos show the slight difference in foliage colour (the broad leaf being a more yellow green) and the long leaf plants are a centimetre or so taller. These plants are about 3 weeks old and grown under identical conditions. The intermediate variety more closely resembles the broad leaf.

Persicara tinctoria

3 varieties of Japanese Indigo at three weeks from sowing.

More Pests

We have found something that eats madder.

Rubia tinctorum pests

This is probably the caterpillar of the Orange Underwing moth, a known pest in the UK which eats a whole variety of plants. So we’re not surprised it’s had a go at our Common Madder. Fortunately there are not enough of them to do any real damage, but they do spoil the appearance of the plants. We can live with that, so no need to take any action.

Suppliers

Rühlemann’s herb nursery has an excellent collection of dye plants and seed for sale and don’t mind sending stuff to other European countries. Their service is excellent.

Poyntzfield Herb Nursery   Scottish herb nursery sells various dye plants and will sell Dyer’s Woodruff root cuttings. Recommended.

References

* Dominique Cardon, Natural Dyes : Sources, Tradition, Technology and Science   . The Definitive reference book of dye plants and dyeing. If you want to know what dye plants are native to the country you live in you will find the information here. A master work, expensive but worth every penny.

Our back garden

Natures Rainbow new plants 2018

The Natures Rainbow Garden 2018 – Part Two, New Plants

By Ashley Walker
Copyright August 2018

Introduction

Since the industrialisation of synthetic dyes most of the knowledge of plant dyes was lost in Europe until it was partially revived by craftspeople like Ethel Mairet and Later Jill Goodwin, Hetty Wickens, Jim Liles, Jenny Dean and many others. Jill Goodwin lists 140 dye plants alone in her book “A Dyer’s Manual”. Reading the books of these trailblazers has given me an almost obsessive interest in some of these plants – how to grow them, how they are related, what dyes do they have in common etc.  In today’s plant dye world we seem to have concentrated on just a handful of key plants (such as Madder, Japanese indigo, and Weld) which give the best and most light fast colours. People still like to try dyeplant materials that are easily foraged and some of these produce good colours, but many are short lived. Personnally I think that foraging in an already over exploited environment is a practice that should be avoided if possible and I want to grow the plants myself, find out more about them, what they look like, how they grow, what sort of conditions they like, how closely related they are, what pests eat them etc. Natural dyeing is a step on the way to connecting with our precious environment and finding out about and growing the plants we use is another step.

Some while back I realised that Common Madder has a host of relatives, some of which are actually native to the British Isles. As you would expect with close relatives, these plants are similar in appearance and habit. They are all clambering or creeping plants with weak, square stems and thin spikey leaves which usually grow in whorls from the stems.

There follows a list of some of the experiences I’ve had with new plants this year starting with relatives of Common Madder. Where possible I obtained seeds and started them indoors in seed trays in March/April, planting out in May.

Dyers Woodruff – Asperula tinctoria

Asperula tinctoria

Dyer’s Woodruff

Asperula tinctoria

Dyer’s Woodruff in flower

I was unable to obtain any seeds for this madder relative so I was very pleased to discover a Scottish plant nursery (Poyntzfield Herb Nursery)  selling the plants. In March, they sent a big bundle of bare rooted plants wrapped in sphagnum moss.  But as we were then still experiencing freezing and wet conditions I potted up the thick red roots in some ordinary potting compost. Most of these have grown well but a few died after initial good growth. There remain a few which are struggling with yellow brownish foliage even though I planted them out in a variety of soil types. I’m not at all sure what the problem is. Dyer’s Woodruff is an attractive feathery plant similar to its relatives with two to four small thin leaves at intervals along its stem. Small white flowers appeared in June. Now in early August it looks as if a tiny few are developing seeds, which I hope I’ll be able to save. The roots are not as large as madder but they are quite respectable and I’m thinking that of all the new madder relatives we obtained this year this is the most promising. The books say it will grow in acid and alkaline soils and can also grow in partial shade. I’m testing this out.

Ladies Bedstraw – Galium verum

Galium verum

Ladies Bedstraw in flower

Galium verum

A clump of young Ladies bedstraw plants will grow into a cushion and then a carpet.

This plant is native to Hertfordshire and happily grows in chalk soil meadows. It will also grow in many other conditions, including poor sandy soils. The leaves are smaller than Dyer’s Woodruff but have whorls of six leaves at intervals along its stem, much like madder. This plant has grown from seed very robustly. I planted seedlings out in clumps of 15 to 20 creating very attractive cushions of feathery green foliage. These have  grown into ground covering carpets with flower stems reaching 6-12 inches high, with tight clusters of pretty yellow flowers in July/August. It makes an excellent trailing plant and although the flowers don’t last long it would make an attractive contrast to some more showy flowers. In the wild this plant is very competitive and will happily grow in grassy meadows. Tended and watered it responds very well, producing long lasting carpets of foliage. Wild plant roots are thinner than Dyer’s Woodruff so I’ll be interested to see if cultivation makes a difference.

Field Madder – Sherardia arvensis

Sheradia arvensis

An agricultural weed, Field Madder, is a small creeping annual plant with thin roots.

This is a classic annual weed of agricultural areas producing small creeping plants with tiny pale pink flowers, leaf whorls of from 4 to 6 leaves looking very much like miniature madder leaves and large seeds which are produced very quickly. It’s difficult to see how this could have been used as a dye plant considering its small size, short life cycle and thin roots. The books say it was used, so I thought I’d give it a try. Seeds are not too difficult to obtain but do not readily germinate – they have a typical weed habit of staying dormant in the soil maybe for years waiting until the conditions are just right. They do produce a mass of roots so it could be worthwhile. I think that the key to obtaining an easy harvest would be to grow it in pots in good quality compost that could be washed away when the roots have grown. I do not know how much of a problem weed these plants are but they do seem to like growing with other plants which they use for support and do not do so well on their own. They are supposed to be good self seeders so we will see.

Devils Bit Scabious – Succisa pratensis

Succisa pratensis

Rosettes of Devil’s Bit Scabious planted around an Alder Buckthorn sapling in a specially created acid soil bed. There are also some first year weld plants bottom right.

Succisa pratensis

Devil’s bit scabious flower

This is a plant I’ve wanted to grow for a long time for its ability to attract bees and other pollinators. In addition, its pin-cushion-like flowers are a pretty lavender blue and open out in July to October at the same time as many of our yellow flowering dye plants. Growing some plants with a contrasting flower colour has been a bit of an obsession for us. Yellow is nice but needs contrasting colours to really bring it out so I was delighted to discover that the Devil’s Bit Scabious is also a reasonable dye plant, at least according to Jean Fraser in her book Traditional Scottish Dyes where she gives a recipe for greenish yellow with alum mordanted material. Intriguingly she also notes that according to Ethel Mairet the leaves of the Devil’s Bit plant also contain indigo, but I’ve read that before about Weld and that turned out to be nonsense.  (I can feel an experiment coming on!).
The plant grows much like woad, producing a thick rosette of large leaves in the first year or two before flowering. It is a perennial but can, according to other accounts, suffer from getting crowded out by more vigorous plants. It is notoriously difficult to germinate from seed – out of about 100 seeds I only managed to get about 4 germinations and, on previous attempts, none at all. Fortunately the plant can be obtained from specialist nurseries and we got some very healthy specimens from Rosybee which have grown very well and two of these have just started to come into flower.

Shrubs and trees

Alder Buckthorn – Frangula alnus

Frangula Alnus

Alder Buckthorn

Alder and Purging Buckthorn are often sold as hedging plants. They can be found growing in the UK countryside provided you know what they look like. And there is the rub! They look pretty much like a whole load of other small trees so part of the reason we decided to buy some saplings was to familiarise ourselves and be able to identify them in the wild. The nursery we bought the plants from (Ashridge Nursaries) were adamant that Alder Buckthorn could not be grown in our chalk soil so I have put  plants in different soils and environments to see how they get on. They arrived bare-rooted in mid March, after the late freeze relented. I heeled them in compost in a sheltered spot on the patio at home until planting them out in April. So far the best growth has been achieved on the allotment, planted in a special “acid” bed made by piling up and digging in ericaceous compost to the light chalk soil. Second best growth is in a large garden planter filled with a mixture of ericaceous and ordinary compost. The last 2 were planted into a cleared grove of Blackthorn growing on chalk soil without any compost, or any watering for that matter. Needless to say these two have not grown much at all, but they are still alive despite the drought and alkaline soil, so we will see. The bark and leaves of this and Purging Buckthorn are usually cited as sources of yellows to dark brown dye stuffs with “sap” green coming from the unripe or ripe berries (different sources give different information). Of the two species, Alder Buckthorn seems to be the main dye plant but I have been unable to find any direct comparison. Another experiment that needs doing!

Rhamnus cathartica and Frangula alnus

Purging and Alder Buckthorn roots are quite different. Black roots of Purging on left and red roots of Alder on right.

Purging Buckthorn – Rhamnus cathartica

Rhamnus cathartica

Purging Buckthorn

Very similar in appearance to Alder Buckthorn but supposedly  equally happy on acid or alkaline soil. I planted most of the saplings on chalk soil at my apiary and left them to fend for themselves. But I saved one sapling to try out in an acid bed, on the allotment (near the Alder Buckthorn) but it has not grown as vigorously and the leaves have gone yellow in places.

Both Purging and Alder Buckthorn are serious invasive pests in the United States and Canada and are banned in two US states.

Black or Quercitron Oak – Quercus velutina

Quercus velutina

Black Oak sapling

This is a large tree from central and eastern USA which became a very important commercial source of yellow dye in Europe in the 19th Century, even after synthetic dyes started to dominate. We have read a fair bit about this tree’s splendid history and that of the man who promoted it (Edward Bancroft – scientist and spy) and thought we would try and grow it mainly out of historical curiosity. Despite a warning found in one dye book that you could not grow it in the UK, we found a supplier in Cornwall (Burncoose Nurseries). So we are now the proud owners of a small sapling growing in a large planter in our back garden. It will be great to see if we can get some dye stuff from the inner bark but, let’s face it we might be long dead by the time the tree is big enough to harvest a branch or two!

Smooth Sumac – Rhus glabra

Rhus glabra

Smooth Sumac in flower

Of all the different species of Sumac, we decided on this North American one for several reasons. It’s perhaps one of the most decorative,  it is wildlife friendly and also fully hardy. It has a high tannin content and the berries it produces are said to be edible. It can produce invasive underground suckers so we are growing it in a large planter. There are plenty of other sumacs growing in peoples gardens and in waste areas around Hitchin but it’s nice to have one right there in the back garden – no foraging needed.

 

 

 

 

 

Hopefully in a year’s time we’ll have some dyed samples to show how successful these new plants have proven to be.

References

Traditional Scottish Dyes  by  Jean Fraser

A book on vegetable dyes by Ethel M Mairet

Edward Bancroft Scientist, Author, Spy by Thomas J. Schaeper

A Dyer’s Manual by Jill Goodwin

Natural Dyes for Spinners and Weavers by Hetty Wickens, A batsford craft Paperback.

The Art and Craft of Natural Dyeing, Traditional recipes for Modern use by J. N. Liles

Suppliers

Rosybee – Plants for bees http://www.rosybee.com

Poyntzfield Herb Nursery  http://www.poyntzfieldherbs.co.uk

Ashridge Nurseries https://www.ashridgetrees.co.uk

Burncoose Nurseries https://www.burncoose.co.uk

Rubiaceae. Rubia tinctorum, Sheradia arvensis, Galium verum and Asperula tinctoria

Ladies Bedstraw intergrowing with Field Madder and Dyer’s Woodruff. Top left is some Common Madder.

Susan Dye and Ashley Walker

The Natures Rainbow garden 2018 – Part one

by Ashley Walker
Copyright August 2018
Banner photograph copyright Sharon Cooper

On the 9th August, after two months with barely a drop of rain, the heatwave and drought in the South East of England may finally have come to an end. Despite regular watering the unnatural weather has taking its toll on our dye plants. For the first time our woad plants are being eaten by Cabbage White butterfly caterpillars (Large White Pieris brassicae and Small White Pieris rapae) and more recently by flea beetles (genus Phyllotreta). I guess the critters were getting desperate to find plants with a bit of juice in their leaves. The weather is having an impact on me as well, I have to water the indigo nearly every day and keeping the rest of the garden needs water too so I’m spending hours each week that I’d rather be spending on writing or dyeing.

This is the first part of a two part post on observations of the dye plants in our garden. This one deals with the plants we have been growing for more than a year. The second part will cover new plants.

European Woad – Isatis tinctoria

Isatis tinctoria being eaten by Large White butterfly caterpillars

These Large White caterpillars managed to eat the whole woad leaf, leaving only the midrib behind.

We have grown Woad for about 12 years now and for the first time our plants have been attacked by caterpillars and flea beetles. This makes a change from the usual small black slugs which put a few holes in the leaves but seldom do any serious damage.

Isatis Tinctoria leaf with eggs and lava of Large Cabbage White butterfly

A cluster of Large White butterfly eggs on the underside of a woad leaf

Isatis Tinctoria being attacked by Flea Beatles

Shiny black small Flea Beatles can slowly chew their way through a woad leaf leaving it like a sieve.

Isatis tinctoria

Woad flower spike August 2018 – from seed to flower in one season as a result of pampering.

I expect that the extraordinary hot weather is to blame with the butterflies and beetles probably acting in desperation. Although the flea beetles appear to thrive, the caterpillars have had a much harder time digesting the unpalatable leaves and most of the newly hatched critters have simply died, leaving a few small holes in the leaf. Only one plant had its leaves reduced to its midrib but even this one will survive as it is now putting out new growth. Interestingly it appears to be only the plants I have watered which are being eaten. There are a few plants which never get watered and these are looking fine.

A few people have asked about growing Woad in tubs or containers and this year we’ve had a few in containers ourselves and this has revealed a problem. One of our plants grown in a container in good compost and watered and fed regularly has grown large and is currently putting out a flower spike which will drastically reduce the amount of indigo in its leaves. Its very unusual to see Woad flowering in August so I can only assume we have pampered it too much – given it the ability to grow large enough to flower in one season. So if you are growing Woad in containers don’t give them too much fuss!

Chinese Woad – Isatis indigotica  

Isatis indegotica

Chinese Woad – about as big as it gets before flowering

Isatis indigotica

Planted out in April these Chinese Woad immediately produced flower stems

We have been growing this for two years now, desperately trying to find out how to stop it flowering a few months after planting. From what I’ve read I’m in good company and this is the chief reason Chinese Woad has not caught on as a source of indigo, despite the fact that it could potentially produce as much dye as Japanese Indigo. Some of the literature indicates that botanists think Isatis indigotica is basically just a variety of tinctoria (European Woad). However, if that is so it has evolved away from tinctoria to a considerable extent. Indigotica is clearly adapted to a much warmer climate and although still nominally a biennial it behaves much more like a half hardy annual. It will flower at any time of year, even in winter, so its rosette stage is always very short and the plant never gets very big. The leaves are a paler blue-green than European Woad and its yellow flowers will continue to be produced throughout the year provided the plants are watered and taken care of. Once the plant starts to flower the larger rosette leaves die off leaving only small leaves on the plant which are probably no good for dyeing. According to the Handbook of Natural Colorants, indigotica will be triggered into flowering if the night time temperature falls below 5°C, which makes it almost impossible to grow the plant to any respectable size here in the UK. Even in Mediterranean climates the plant can only usefully be grown in the Summer. From my experience the plant will flower even if you just look at it the wrong way so I’m coming to the conclusion that it’s not worth the effort. It does grow very quickly however and if you were to grow it en masse and harvest the leaves before it flowered it might just provide a return for your efforts.

Another problem with Chinese Woad is its susceptibility to pests. Caterpillars and aphids like it very much and can easily destroy your plants.  And you guessed it, significant insect damage will also trigger flowering. In a mad moment I decided to see if Chinese Woad tasted any nicer than European Woad. But the taste test settled nothing, both plants are extremely bitter and fiery. I obviously don’t have the finer tastes of Cabbage White butterfly caterpillars!

Japanese indigo – Persicaria tinctoria

Persicaria tinctoria - Long Leaf variety

Long leaf variety of Japanese Indigo with curled leaves to protect itself the prolonged hot sun of 2018

This year we are growing the same three varieties as last year – Long Leaved, Broad Leaved and an Intermediate Leaved white flowered variety. There appears to have been no interbreeding from last year. This year the difference between the long leaf and broad leaf varieties is stark. The Long Leaf plant is very vigorous with dark green leaves. The Broad Leaf variety took a long time to get going as usual and suffered from its leaves turning red. I was initially confident that the red colour was partly due to the hot sunny weather we were having in early summer – the slow growing plants were getting roasted. But after a good feed (with chicken manure pellets) the plants started growing quickly with the new foliage a nice mid green despite the continued hot sunny weather. So a bit of a chicken and egg situation: was it the lack of fertilizer that caused the leaves to redden or simply that the young plant leaves, growing slowly, were getting a longer exposure to the hot sun?  The Long Leaf variety reacted differently to the hot sun with leaf curling , something I had seen last year but only on plants grown in the greenhouse.

Persicaria tinctoria

A bed of intermediate White flowering Japanese Indigo.

Persicaria tinctoria

Newly planted out Broad Leaf Japanese Indigo with sun reddened leaves.

Thus far we have only harvested the Long Leaf variety and used it in a little experiment comparing Jenny Dean’s extraction technique with the more often used long soak in cool water. The results will be written up in a later post. What I have also noticed is that we are currently getting a considerably better production of indigo from Woad than the Long Leaf variety of Japanese Indigo. Woad is well known for giving better results when the weather is hot and sunny. If the climate change predictions are correct and we continue to have hot summer weather then I think we would be better to return to growing mostly Woad. The Long Leaf variety of Japanese Indigo produces the least amount of indigo dye of the three varieties (see comparison here) but it does produce larger plants so perhaps still produces an equivalent amount of indigo per square metre.

Madder – Rubia tinctorumRubia tinctorum berries

Once again this year the madder plants are producing masses of berries. This is the third year running. In the previous 10 years or so the plants produced only a few. I have no explanation as to why this is.  I’ve grown plants in different soil, in planters and in the ground and all plants are doing the same. A result of the weather?

Rubia tinctorum

Madder plant obtained from Southwark Cathedral in early 2018.

This year we obtained a new madder plant sourced from Southwark Cathedral dye garden. The plant is quite different to plants I have been growing up to now (all of which were derived from a single seed over 10 years ago). This new plant has paler leaves with a different shape and it flowers about 3-4 weeks later. It will be interesting to see if the root yield is also different. I’m pleased to have been able to increase the genetic diversity of our madder as I’ve always propagated by root stem cuttings or from seeds from my own plants.

Wild Madder – Rubia peregrina

Rubia peregrina

Wild Madder in flower – Early July

We’ve been growing this plant for nearly three years now. It’s an evergreen but the tops do not appear to be totally hardy in the UK climate and were damaged by the winter frosts. This is the first year in which the plants (originally obtained from a wild flower nursery) are starting to look a bit happier. They are putting out new shoots from underground stems and flowering for the first time. It remains however a very slow growing perennial and I think it will take longer than Common Madder to produce a good root harvest so we are leaving it for another year.

I was given some seed from a friend from some wild plants growing on the south west coast which nearly all germinated though it did take well over a month before the first shoots appeared.

Saw wort – Serratula tinctoria

Serratula tinctoria

Saw-Wort plants with yellowing of leaves.

Serratula tinctorum

A self seeded plant with dark green leaves growing next to the transplanted ones with yellow leaves.

This native  plant continues to be disappointing. Not only do the plants remain small but about half of them suffer from bad yellowing of the leaves once planted out in the garden. I have tried practically everything to remedy the problem – fertiliser, Epsom salts and seaweed extract. There are some self-seeded plants which look very healthy so I do wonder if the roots are somehow getting seriously damaged during transplanting. It also remains likely that there is something wrong with the soil itself as other plants (Genista, a red scabious and a Purging Buckthorn shrub) are similarly affected.

Serratula tinctoria dye comparison

A comparison of our main yellow dye plants. Top is Weld, Bottom Right is Genista and Bottom Left is Saw-Wort

We did try dyeing with the Saw Wort this year and obtained a good buttery yellow. We were hoping it would be a nice lemon yellow like Weld and Genista so were a bit disappointed with that too.

Dahlia species

Dahlia Species

Bumble bee on single type dahlia grown from seed.

Dahlia Species

Dark Red Dahlia giving pinky purple and greens. Possibly “Nuit d’Ete” or “Black Cat”

The colour of Dahlia flowers has an effect on its dye but we did not appreciate by just how much until this year when we tried using some deep red flowers to dye with. We obtained nothing like our accustomed strong yellows with acid pH and strong orange with alkaline pH. This time we got green with alkali and blue/purple with acid indicating that the dyes in this dark red flower were the same as you find in red cabbage and some other red flowers. These dyes, although very pretty, are not light fast. Over the years of growing Dahlia we have narrowed down the varieties that produce the best results for the home dyer. These are yellow or orange double flowering pom pom types. The pom pom flowers are longer lasting and produce more dye – some pom poms are very large and yield a lot of dye but bees and pollinators are unable to assess the nectaries. We have tried to stay away from these but there’s no doubt they are the best for dyers.

Tansy – Tanacetum vulgare

Tanacetum vulgare

Tansy needs regular watering for healthy plants.

Often used by Scottish dyers as a source of yellow dye this plant has been growing in our garden for several years now but largely unused because the plant wasn’t very vigorous. There was never enough plant material to harvest and the flowers were disappointing. This year we planted a bed of Japanese indigo alongside so the Tansy benefitted from being regularly watered. The resulting Tansy flowers have been lovely so if you’re growing them keep them watered for best results.

Perennial Coreopsis –  Coreopsis grandiflora varieties e.g. Golden Joy, Sun Ray, Early Sunrise

Coreopsis grandiflora

Perennial coreopsis – plant breeders benefitting the plant dyer.

Coreopsis grandiflora

Bright orange on alum mordanted wool blanket.

These are double flowering perennials with deep orangey yellow flowers which produce a lot of dye. They are not as hardy as the growers would have you believe as half our plants died during the winter and only a few have recovered enough to put on a good show this year. However, many can be easily grown from seed so are not too expensive to grow. They make excellent bedding plants and produce a fabulous orange dye from the flowers. An example of the plant breeders unwittingly aiding the home dyer.

Dyer’s Alkanet – Alkanna tinctoria?Alkanna tinctoria

Alkanna tinctoria

Alkanet root. Bottom tip has had thin outer black bark removed revealing the dissapointingly white root.

This is the third year of growing and though I have not tried to extract any dye from its roots I am deeply disappointed to find that the roots are not red as they should be. I was suspicious as soon as I started to grow the plant from seed bought from the German Company Rühlemann’s. The plant seemed too vigorous with over large leaves and not hairy enough, but I persisted with it until it flowered. The flower shoots were tall (up to about a metre high) and not at all like the creeping wild flower growing around its native Mediterranean. The flowers when they finally appeared were the only part of the plant that looked like the pictures of Alkanna tinctoria seen all over the internet but the roots? The roots were white!

Doing some reading around this ancient dye plant I find that its qualities as a medicinal plant derive solely from the coloured substances in the root which were used as a dye, cosmetic and bio stain so you can imagine the way I feel after lavishing attention on this plant for the last three years only to find the roots are white! Recently I discovered one internet comment on the plant that says the cultivated version of the plant does not produce as much dye as the wild type. Well that’s some understatement. Of course it is possible that lavishing attention on the plant was entirely the wrong thing to do and I should have left it alone but it seems more likely that the growers have simply selected the seed year after year from the largest prettiest plants and in so doing have bred out the qualities that gave the plant its historical value.

Just to confuse matters Alkanna tinctoria has been and is also known as “Anchusa bracteolata, Alkanna tuberculata, Alkanna lehmanii, Lithospermum lehmanii”, and has been given various common names as follows Alkanna Radix, Buglosse des Teinturiers, Dyer’s Bugloss, Henna, Orcanète, Orcanette, Orcanette des Teinturiers, Orchanet, Radix Anchusae. Rühlemann’s who sell the seed are now calling it Alkanna tuberculata. There is certainly confusion on the identity of all these plants. Are they all the same or not. If there are any botanists out there  who can get to the bottom of this please please get in touch!

References

Philip John and Luciana Gabriella Angelini – Indigo – Agricultural Aspects. Chapter 7 of Handbook of Natural Colorants  Edited by Thomas Bechtold and Rita Mussak. Wiley Series in Renewable Resourses. (Available as free download).

Rühlemann’s  This German herb plant and seed supplier has a number of dye plants for sale including Chinese Woad and Long Leaf Japanese Indigo but it is primarily interested in the medical properties of the plants it sells and I get the impression they know little about plant dyeing.

The Natures Rainbow Year – (and its only half way through!)

An article by Susan Dye and Ashley Walker
© copyright 2018

2018 is turning out to be our most successful yet.

The year began with our good friend Brian Bond joining us to deliver a two day workshop in Ipswich in late January with the International Felters Association (see above). Susan was involved in much mordanting in preparation. This was our second major plant dye workshop away from home, and dependent on friends or family to help us with transport. Hard work packing an ‘all singing all dancing’ workshop and the three of us into a single hatchback vehicle (albeit a large one, thanks Brian!). Quite stressful but very well worthwhile, as the students were terrifically motivated and created a full palette of wonderful colour on the finest merino tops.

Also in January we had confirmation that Southwark Cathedral had invited the London Guild of Weavers, Spinners and Dyers (WS&D) to demonstrate plant dyeing as part of London Craft Week in Mid-May. Susan was asked to coordinate the project, having held a successful mini natural dye demonstration there as part of the biennial London Guild exhibition last November.

Preparations for all this activity took place mostly in the winter and early spring when the weather was too cold or wet to work outside on the dye garden

In between scoping and planning the London Guild event at Southwark, Susan gave talks on plant dyeing to the Chelmsford Embroidery Guild, on the red dye from madder for the Cambridge Guild of Weavers, Spinners and Dyers and, closer to home, a talk on the horticulture of dye plants for the Wymondley Gardeners Group. Had the snow in early March not intervened there would have been another talk on the history of Norwich Dyers to region 7 of the Quilters Guild.

London Craft Week event at Southwark Cathedral with the London Weavers, Spinners and Dyers Guild

The Shard overshadows our colour splash at Southwark Cathedral

Susan spent much of April mordanting and test dyeing fabric and yarn for the London Craft Week event, which was to be held outdoors in the Churchyard in mid-May. Fortunately the weather improved and we were blessed with two sunny breezy days. With help from textiles graduate Hannah Sabberton, Susan and I carried Hitchin grown fresh woad and dry Weld, Indigo dye solution, mordanted fabric yarn and fleece, samples, display materials and goodness knows what else (kitchen sink comes to mind!) on the train and bus into Central London at rush hour. We are resourceful public transport travellers with trolleys and backpacks and all arrived safely! Mercifully all the pans and heaters had been supplied by London Guild members based not too far away (thanks to Penny and Diane). Also there were many, many lovely dyers from the Guild who shared the demonstrating. All told there were twenty two volunteers across the two days. We spoke to people from all over the world, from London and other parts of the UK. Tiring but very satisfying to see the rainbow of colours we achieved with just the three medieval ‘grant teint’ plant dyes: Madder, Weld and Woad.

Susan managed to escape a couple of times down to the British Library where she loves to do research on the history of dyeing and in particular the 19th Century “Norwich Red”. An article to be published in the Autumn issue of “The Journal of Weavers, Spinners and Dyers” will detail her findings so far. We have also been asked to write an article on growing dye plants with a particular emphasis on small gardens and container growing. This should appear in the next issue of “British Fibre Arts” along with a profile about ourselves. The Editor Rainy Williamson made us think about what we do and why we do it. I was particularly reminded that many people do not have access to a garden or allotment and may only be able to grow dye plants in small spaces. I immediately set about making and planting up some large-ish containers with suitable dye plants to see how they responded. And then we got to thinking that apart from a couple of small demonstrations and the regular workshops for our local guild we’ve never made an effort to share our skills in plant dyeing with the local population. So Susan quickly got on the phone and asked the Hitchin Festival organisers if they still had some slots left in their programme and lo and behold, (thank you Keith)  we were found a slot in the programme.

Indigo Blue, Weld and Chamomile yellow and Greens produced by overdying yellow with blue and blue over yellow

Results from the green overdye experiment done at the Herts Guild of Spinners Weavers and Dyers Workshop

Meanwhile we had another workshop for our local Guild in North Herts to get ready for. This was based around an experiment investigating the notion that a better green is obtained if wool is dyed first with indigo and then weld (yellow) rather than the other way round as we have traditionally done it. Various accomplished plant dyers had reported this finding and we wanted to check it out. The workshop produced some fantastic greens and, somewhat to our surprise, the blue overdyed with yellow did indeed produce the best green.

While all this has been going on I’ve been working hard on the Natures Rainbow dye garden, getting it into shape to satisfy the North Herts District Council allotment inspector (Grounds Maintenance Monitoring Officer). Because we are growing a most unusual set of crops some of which look remarkably like weeds we

Rubia tinctorum

Madder is closely related to the weed Cleavers or Goosegrass. It looks and behaves much the same but is altogether larger in stalk and leaf and has berries instead of hard seeds.

Ransoms Rec Allotments, Hitchin

The Natures Rainbow allotment plot in early June.

have to make the plot look as tidy as possible. Madder for example is a close relative of the weed Cleavers and has the same sprawling habit and Weld is generally classified as a weed anyway. In addition, we leave our second year Woad plants to go to seed, so we have stock for the following year and this too raises eyebrows.

Asperula tinctoria

Dyers Woodruff in flower

We also decided early on this year that if we are going to continue giving talks and writing articles about growing dye plants then we need to expand our experience and grow some of the more unusual dye plants so we sent off for more seeds including Chinese Woad, Wild Madder, Field Madder, Ladies Bedstraw, Blood Root and where we couldn’t get seeds we ordered plants. These include Dyers Woodruff, Black Oak, and Smooth Sumac (Rhus glabra).

Quercus velutina

Our new Black or Quercitron Oak Sapling. The inner bark of this North American tree produces the dye quercitrin which for a while was a major industrial source of yellow dye. Of course it will be many years before we can harvest any bark from this specimen!).

Reseda luteola

Honey bees are particularly fond of Weld

 

 

 

 

 

 

 

 

As a beekeeper I’m also very interested in growing plants that are also good for all kinds of bees so I’ve been very gratified that many of our dye plants are also fantastic bee plants too, Weld and Japanese indigo are two of the best.

Rhus Glabra

Smooth Sumac from North America, the dried leaves of which contain 25-27% by weight of tannins.

Look out for more blogs detailing some of the events mentioned here but you might have to wait until things calm down a bit before we get time to write them!

Inula helenium

Elecampane – Inula helenium

An article by Ashley Walker
© copyright 2018

When we first became interested in growing and using dye plants we came across an entry in “Traditional Scottish Dyes and how to make them” by Jean Fraser. This seemed to us to be very exciting because it offered a tantalising alternative blue dye to Woad indigo.

Traditional Scottish Dyes and how to make them by Jean Fraser

Page 69 from Jean Frasers book – Traditional Scottish Dyes and how to make them.

Traditional Scottish dyes and how to make them by Jean FraserWe immediately set about obtaining some seeds which were readily available as Elecampane is a popular garden flower and ancient medicinal herb. Our first lot of seedlings were all eaten by slugs but the second batch (protected until they were larger) survived to produce two small beds.

It took a number of years for the plants to reach full size but by this time we had realised that the likelihood of obtaining blue from the roots was very unlikely and we had discovered Japanese Indigo so did not think it worth even trying. We kept the plants because every year we are rewarded with a sunny display of glorious yellow flowers which act as magnets for bees of all kinds. These tall plants with giant leaves are low maintenance and just take care of themselves.

Inula helenium

Honey bee on Elecampane flower.

The Dye garden has grown over the years and we are getting to the point that every plant species we grow has to justify its presence by being a proven source of plant dye. But still, the mystery of Jean Fraser’s entry stuck in our minds so this year I decided to give it a go before the plants started to grow.

Three of the incomplete “no details or quantities given” recipes mention whortleberries and one recipe Elder (presumably berries) as additives to improve the colour. We know by now that most black berries can give pinks, lilacs and mauves with a good alum mordant but they are not lightfast, iron mordants are best at prolonging the life of fugitive dyes and the fourth recipe mentions iron so we thought it worth obtaining some whortleberries . What are whortleberries?

Wikipedia suggests they are one of three possible members of the Vaccinium family:

Vaccinium myrtillus, bilberry, or blue whortleberry
Vaccinium vitis-idaea, lingonberry or red whortleberry
Vaccinium uliginosum, bog whortleberry/bilberry

All three plants grow commonly in Scotland but we think it is a reasonable guess that the name refers to the bilberry V. myrtillis or uliginosum as vitis-idaea is a red berry. The closest source of berries we could get hold of were supermarket blueberries (probably Vaccinium corymbosum). Not as good as our native bilberries as they only have a blue black skin and internal pale green flesh. Our native species are blue/black throughout.

Experiments

Initially we tried a number of variations:

  1. Fresh chopped and bruised roots heated with and without blueberries
  2. Fermented chopped and bruised roots with and without blueberries
  3. Samples of unmordanted, alum mordanted and iron mordanted wool were added to each of the dye pots (the root and berry material were not removed).

The roots of elecampane are white with a yellowish skin and black bark which is not attached to the root and is easily washed off. There appears to be no colour in the root at all!

Inula helenium

Elecampane root

Inula helenium

Elecampane cut root

Because of this lack of colour we had long suspected that the only possible source of colour would be from tannins in the root reacting with the iron mordant to give a grey. We suspected that in Scotland grey was often called blue and with the addition of some whortleberries a bluish grey could be obtained though it would fade to grey over time. As there are many other sources of tannin in the dye plant world we were sceptical that Elecampane root would give us anything worth having.

Results

The results were fairly conclusive in that the only significant colour change occurred with the iron mordanted wool where a silvery grey was obtained from the fresh root and a yellowish grey from the fermented root. The unmordanted wool stayed white and the alum mordanted wool turned a very pale yellow. The addition of blueberries made little difference.

Inula Helenium dyed wool

Right: iron mordanted wool in fresh root dye bath. Left: Iron mordanted wool in fermented root dye bath.

Inula helenium treated woth iron mordant

On the left cut root treated with iron mordant. On the right untreated root.

Painting an iron mordant solution onto cut plant material usually shows up the presence of tannins fairly rapidly but sometimes it takes a few hours to get a colour change. The elecampane root had to be left overnight before the change seen here on the left took place. Other additives mentioned in the recipes are salt and ash. Dipping a cut root in salt had no effect but adding a tiny amount of sodium hydroxide (an alkali in wood ash [lye]) to the cut root turned it immediately yellow and after 24 hours a yellowish dark grey. We did not use any of this alkali in our experiments as we were particularly interested in obtaining a neutral or blue grey but it looks like adding the alkali could aid in getting a darker colour.

Once we were happy we could get this neutral grey we went ahead with dyeing a large skein of hand spun yarn (about 100g) mordanted with 1g of ferrous sulphate*. This was added to a dye bath made from about half a kilo of chopped and bruised Elecampane root heated to around 90°C and left for one hour then strained to remove the solids.

Inula helenium dyed wool

100g skein of hand spun iron mordanted wool dyed with Elecampane root.

OK, so no blue, but a good neutral grey is hard to obtain as most tannin rich plants have additional dye stuffs and the greys obtained are tinted with yellows or browns. Elecampane is almost free of any of these contaminants. As any designer will verify grey has the ability of amplifying adjoining colours making them seem brighter than they really are. A dye garden without a source of grey would not be complete so the Elecampane stays!

Inula helenium

Elecampane in full flower

*The iron mordanting is done according to Liles method using the same quantity of oxalic acid as ferrous sulphate. The Oxalic acid prevents the iron from oxidising from the yellow-green ferrous sulphate to orange ferric oxide (rust).

References

“Traditional Scottish Dyes and how to Make them” by Jean Fraser. Illustrated by Florence Knowles. © 1983, 85 and 96.

“The Art and Craft of Natural Dyeing – Traditional Recipes for Modern Use” by J. N. Liles. © 1990

From Seed to Stitch

best stitch smaller

I am passionate about working with cloth and yarn dyed from plants you have grown yourself.
I gave a talk yesterday to the Chelmsford Embroiderers’ Guild.
I had a lovely evening. Thanks to Angela and June for inviting me and for your hospitality.
As follow up, here are some pointers for supplies and books I promised to share online.

References

Mordants and Natural Dyes
Earth Hues for extracts
George Weil  for plant dyes and mordants; especially aluminium acetate mordant for silk and vegetable fibres
P&M Woolcraft  very friendly and good prices
Wild Colours sells woad powder, dyes and provides lots of information
Fiery Felts  I forgot to mention this supplier in the talk but Helen is very good for dyes especially dried flowers hard to obtain elsewhere. Her booklet on indigo is also excellent.

Dyed threads as well as dyes and mordants
Renaissance Dyeing – based in France
Mulberry Dyer run by Debbie Bamford, a pre-eminent historical dyer who sells at re-enactor markets and also via etsy shop.

Books and blog

Jenny Dean  Doyenne of Natural dyeing in UK. Her landmark book is Wild Colour (2010) but all her books are excellent.

Women’s Work: The First 20,000 Years Women, Cloth, and Society in Early Times (1996) by Elizabeth W Barber

The Story of Colour in Textiles (2013) by Susan Kay-Williams

Exhibition
Fitzwilliam Museum Cambridge Sampled Lives till 7 October 2018

 

Persicaria tinctoria

Three strains of Japanese Indigo tested and observations on indigo extraction

An article by Ashley Walker
© copyright 2017

This year I had planned to carry out a tightly controlled experiment to look for variation in the amount of indigo produced by three fairly distinct strains of Japanese indigo. However due to a prolonged and still undiagnosed illness, my plans were thwarted and the experiment did not work out quite as I had hoped. However, on 12th and 13th October 2017, with help from Brian Bond another keen plant dyer, I did manage to complete a test of the three plants although the results are not directly comparable due to different planting times and maturity of each variety.

The strains

Broad or Rounded leaf indigo

Persicaria tinctoria

Round or wide leaved Indigo. Directly sown bed

Grown from seed originally from the USA (from fellow natural dyer Pallas Hubler in Washington State on the west coast) who sent a few seeds over to Brian in 2013. We have been growing and saving seed from this strain ever since so it is possible that it has become adapted to growing in our soil.

  • Late flowering (October into November)
  • Pink Flowers
  • Compact short flower stems
  • Wide short or rounded leaves
  • Foliage pale to mid green
  • Easily damaged by high nitrogen levels in the soil. Grows poorly in cool overcast weather.

Long leaf indigo

Persicaria tinctoria

Long leafed Japanese Indigo in full flower.

Seed for this was obtained from the German supplier Rühlemann’s. Unfortunately this was in full flower by the time I was able to harvest it for the test and from previous experiments I know that once indigo has committed itself to flower production the amount of indigo in the leaf falls dramatically.

  • Large long pointed leaves
  • Pink flowers
  • Long delicate flower stalks
  • Early flower (September-October)
  • Dark green leaves
  • Very tolerant of high nitrogen in the soil and generally more robust.

An in-between white flowered strain

Persicaria tinctoria

Intermediate white flowered Japanese Indigo

Persicaria tinctoria

Intermediate strain of Japanese Indigo with white flower.

The seed was obtained from Lisa George Fukuda a fellow plant dyer in Guernsey who had it originally from Teresinha Roberts at Wild Colours

Unfortunately this was planted out late in the year (August) so as yet I know little about its habit as there has not been enough time for it to grow to full maturity.

  • Longish leaves
  • White flower
  • Easily damaged by high nitrogen fertilizer.
  • Mid green leaves
  • Quickly bushes out, highly branching.

All three strains were grown on the Natures Rainbow allotment in Hitchin in a chalk soil with a strong application of Fish, Blood and Bone plus some chicken manure pellets.

Persicaria tinctoria

Leaves from all three strains.

Persecaria tinctoria

Rounded leaf Japanese Indigo growing with the Long Leaf strain in the greenhouse. Here they look like two completely different species.

The experiment

After stripping the leaves from the freshly cut indigo stalks, 220g of leaves from each strain were slowly heated from room temperature to 80°C in stainless steel pans with 4 litres of tap water. The pans were stirred at short intervals throughout. Note: the weight of leaves was determined by the amount of the long leaved strain that I could harvest from shoots that had not yet come into full flower as I wished to minimise the effect of flowering on indigo production. The amount of water in the pans was deliberately large as I wished the final colour to be on the pale side as variations in pale colours are easier to distinguish. More water also means the pot is easier to stir before the leaves are cooked.

Heating to 80°C took about 35 minutes. The pans were then taken off the heat and allowed to cool, free standing in the air for 1 hour. (The air temperature was appoximately 20°C).

Persicaria tinctoria

Intermediate Japanese Indigo extraction bath with container of liquor to show gray colour. Photo taken just after pan was removed from the heat.

At this point no difference could be noticed between the different pans. The liquor in each pan being a pale greyish blue in each case.

After one hour the leaves were removed by straining through an old pair of tights into a large plastic bucket. Half a cup of household ammonia was then added to the liquor. Taking care not to breathe in hot fumes, this liquor was poured back and forth from bucket to pan 10 to 15 times to aerate and oxidise the indigo precursor to indigo. The colour of the liquor changed from grey to yellow green, with the round leaved plant giving the darkest colour change and the long leaved plant the least. This is a good indicator of how much indigo is present in each pan.

Once oxidised to indigo, the liquor is now in a stable form and can be left for long periods without any loss of indigo. The reduction vats (indigo dye baths) were set up the following day as follows. The pans were heated to 50°C, one level teaspoon of Spectralite (Thiourea Dioxide) was added to each pan, gently stirred in and left for 30 minutes for the indigo to reduce to its soluble form. Identical weight skeins (26g) of wool were added to the baths at 50°C and left for 20 minutes before removal and oxidation in the air. The dye baths were kept in a hay box to maintain constant temperature during the dyeing.

The results

Japanese Indigo

First results showing a surprising difference in colour obtained

The long-leaved plants (left) were disappointing only producing an ice blue colour. The white-flowered intermediate-leaved plant gave a slightly deeper shade but still pale (centre). The round-leaved plant produced a respectable light blue (right).

The poor results for the long-leaved plants was understandable because of their flowering state, however I was surprised the colour was quite so pale. The good results for the round-leaved plant was a real surprise as I had become convinced these plants would not be the best. Overall the pale colours made me worry that I had not optimized the process and I decided to repeat the experiment for the round-leaved and intermediate-leaved white-flowered plants (I had no more of the long-leaved plant so I could not replicate this one).

On the second run I made one change which was to slow the cooling of the extraction bath after reaching 80°C by placing the pans in hay boxes. For this experiment, using 4 liters of water I was aware that this small amount of liquor would cool quickly, perhaps too quickly? An experiment we conducted some years ago revealed that premature cooling of the extraction bath resulted in a dramatic loss of indigo when processing woad leaves. Two years ago we discovered that leaving the bath at a high temperature for more than one hour also results in a loss of indigo so I have become wary of putting large baths in hay boxes which are capable of maintaining a high temperature for hours.

In this second run the results from the white-flowered intermediate-leaved plant improved but the round-leaved plant still produced the better result (which itself was no better than in the first run).

Skeins of wool dyed with Japanese Indigo

Second run with intermediate white flowered indigo plant compared to rounded leaf plant.

Skeins of wool dyed with Japanese Indigo

Comparison of intermediate white flower strains. The difference between quick and slow cooling of the extraction bath.

Wool dyed with Persicaria tinctoria

No real difference between runs for the Rounded leaf strain.

Discussion

In theory all three plants should have produced broadly similar amounts of indigo. That they did not could have been due to genetic differences but as noted above all three plants were at different stages of development having been planted at different times and the round-leaved strain had possibly adapted to the local soil over the 4/5 or so years I have been growing it. The poor results from the long-leaved plant may have been entirely due to their flowering state. The intermediate-leaved white-flowered strain had only been planted out in late August and may not have had sufficient exposure to the sun to develop much indigo.

The diversity of results shows how critical it is to grow and harvest the plant at the right time. I was certainly concerned that harvesting the plants in October was a risk, as all three varieties were producing flower buds (although only the long-leaved plants were in full flower). Later I extracted a concentrated bath of indigo by making up a large pan crammed full of leaves and only enough water to barely cover the leaves when they were pressed down forcibly. The results were pleasingly strong indicating that the leaves were still fully charged with indigo.

Skein on right dyed with a strong indigo dye bath

Skein on right dyed with a strong indigo dye bath

I will certainly be making strenuous efforts to continue to save the seed from the round leaf strain whatever the reasons for the underperformance of the other two strains!

Confirmation of results

Since this post Leena Riihelä writing in her blog (see Riihivilla) has confirmed that the long or pointed leaf variety of Japanese Indigo does not produce as much indigo as the broad or rounded leaf variety. Leena who also grew three strains of Japanese indigo this year also speculates that the broad leaf (rounded) variety originated in Japan. (The long leaf variety may come from Northern Japan or China). She is also able to confirm that the long leaf variety flowers much earlier. Leena is based in Finland which has such a short growing season that the rounded leaf variety does not have time to produce seed. Leena has a wealth of experience to share about indigo and other natural dyes so please visit her blog and web site. (see below)

Thanks to:

Brian Bond
Leena Riihelä at Riihivilla
Lisa George Fukuda
Pallas Hubler

Indigo dyed wool

The range of blues obtained from the three strains of Japanese indigo.

Madder Red by Robert Chenciner

Looking into Chenciner’s Madder Red

An article by Ashley Walker
© copyright 2017

Madder Red – A history of luxury and trade (2000) by Robert Chenciner
published by Curzon Caucasus World ISBN 0 7007 1259 3

This book is devoted to all aspects of the history of madder from cultivation, through process, economics and use of dye and pigment. The author has collected together in this one reference work the result of many years research.  It is a mine of information. The book is not a light read and the first time I was able to get hold of a copy I only read the chapter on madder cultivation which I found of particular interest. Since obtaining our own copy I have discovered the book contains many additional snippets of information on cultivation and use which compliment our earlier article (see here). My interest, from the point of view of the small scale grower and crafter, covers those aspects of growing and using madder that could be employed on a domestic scale. In the remainder of this article I attempt to extract information of practical use (see comments in Red).

The Madder Plant

The book contains information collected from multiple sources from all over the world but chiefly from the Caucasus and Russia. The focus is mainly on Rubia tinctorum  but other plant sources of red dye are also noted, particularly Rubia peregrina (Wild Madder) which was used quite often when tinctorum was not available. The roots of peregrina contain purpurin and little or no alizarin. Purpurin was valued for producing superior pink and violet shades.

Plant diversity, propagation and seed fertility

In different places madder appears to be adapted to local conditions and taking seed or plant material to grow in other parts of the world often resulted in failure – though this may have been due to inexperience of the new farmers. The book also confirms my own experience that the seed of madder is difficult to germinate and can easily become infertile due to poor storage.

For the home grower this means using the seed as soon as possible (within a year of harvest).

Farmers invariably preferred to sow seeds direct but only the most experienced could do this with success. New farmers preferred to grow the seeds in nurseries and then transplant into the fields when big enough or take rooted shoots from a field being harvested. Transplanting was harder work (and so more expensive) but ensured a greater chance of success.

Crop rotation, maintenance and soil fertility

Maintenance

Six months after planting, the rows of madder plants were “earthed up” (like potatoes) to encourage the plant to put out side shoots (underground stems) and protect the plant from drought in the summer and hard frosts in the winter. This practice is also reported as improving the quality of dyestuff.

For the home grower this seems a sensible activity if you like to grow madder in rows as it would allow the roots to be more easily dug out.

The main maintenance job is reported as weeding, with the most difficult weed being couch grass. I have to agree with this as couch grass has a very similar habit to madder and also forms a mat of underground roots which are extremely difficult to untangle once they get a grip.

Crop rotation and soil fertility

Most of Chenciner’s references to soil fertility indicate that madder harvests (weight of root and quality of dyestuff) will decrease over several years if grown in the same soil continuously – even if the soil is well fertilised with manure. A figure of approximately 6 to 12 years is mentioned as the maximum length of time that madder could be grown economically in the same field. After this time the land had to be left fallow or rotated for several years (4 to 12) before any further madder crops could be grown. Typical rotational crops were rapeseed, beans, wheat, hemp, turnips, beet, potatoes and cabbage.

Several references are made to observations that madder grew best on virgin ground which is much the same as any other crop, but the failure of manure to restore fertility suggests a depletion of some micro-nutrient not present in manure. The only suggested method of restoring fertility quickly was to add “natron” and common salt. Natron is a mixture of hydrated sodium carbonate salts and other salts found in dried up lakes.

For the home grower it may be possible to substitute common washing soda for natron but I would not recommend doing so without careful experiment first to find out how much to apply. Washing soda is a powerful alkali and sprinkling it on soil could do serious damage.

Adding small quantities of sea salt (35g per m2 about twice a year) may be a better solution but be careful not to overdo it. Rock dust may also do the job.

How long to grow the plant before harvest?

Throughout its history this subject has been the source of much discussion and the author comes to two conclusions:

  1. Older roots (3 to 5 years) produce the best quality dyestuff.
  2. Economically it was best to harvest after 1 to 2 years.

As you can imagine 3+ years is a long time to wait before being paid, particularly if as an “adventurer farmer” you had to pay rent on the land/accommodation and feed a family during this time. Most successful ventures appear to have been run by established land owners who had minimal overheads and additional sources of income. Some farmers did practice a form of partial harvest where a trench was dug beside the row of madder plants. Roots found in the trench were harvested without killing the main plants which continued to grow for a further year or two.

This practice makes home growing of madder considerably less of a wait though the final harvest may be reduced.

Harvest and processing of madder root

Steaming

The first procedure after digging the roots was to steam them, a practice carried out in the field by a team of specialists. All sources are clear that this process increases the amount of dyestuff in the root and after about 4 to 5 hours the roots would turn from yellow orange to a strong red. A hole was dug in the ground and a fire lit. When the surrounding soil had become baking hot, madder roots were piled on top and then the whole heap was covered in damp cloth or similar material to keep the hot air in.

Although we have never tried this I see no reason why it would not be possible to do this at home using standard vegetable steamers. The exact method will need to be worked out by experiment.

Washing

There are very few reports of root washing in the book and when it is mentioned it is not recommended for fear of loss of dyestuff. I would guess that the growers wanted to keep even the poor quality brown dyes found in the thin skins. Any soil clinging to the roots would just add to the weight of the final product, so more profit!

Drying

In the Netherlands and Britain this was done in specially built heated drying houses as the climate here was not hot enough to dry outside. Even in the Caucasus and other hot dry areas most growers preferred to dry in the shade rather than direct sun. This slow drying is reported as another essential process to further increase the amount of dyestuff in the roots. Roots were often stored for one or more years to allow them to mature before being pounded into a fine power or “krap”. The roots had to be brittle dry before pounding otherwise the root would stick into a hard cake.

For the home grower the important features of this drying process is the temperature and the length of time. The recommended temperature was between 20°C and 30+°C so drying in an airing cupboard would probably work well with storage in a warm dry place after the roots have dried out completely.

Fermentation

Fermentation was sometimes done before pounding, sometimes afterwards and involved placing the root material into a vessel with water for a short time (a few days) during which time the sugars in the root were fermented out. Removing the sugar was important as later fermentation in the dye bath interferes with the dyeing process.

From the home dyer’s point of view this is not so important unless you make your madder dye bath a day or two before using it.

Pounding

When the madder industry was in full swing the roots were pounded in large horse-powered or water-powered mills and the resulting powder or krap was sorted into a variety of grades. The main problem besetting the root processors was separating out the “tough” outer skin which contains the brown dyes that would dull the final dyed product from the inner “parenchyma” part of the root which contained most of the dyestuff. Exactly how this was done is not explained but logically krap was probably sieved into coarse and fine fractions and the first powder produced after partial pounding would have presumably contained most of the bark.

For the craft dyer pounding is not really an option. It may be possible to grind the root in coffee bean grinders but only if you are prepared to say goodbye to the grinder. The metal blades in such grinders could be a problem if they become rusty and end up adding iron to the dyestuff which would sadden the colour. Chenciner reports that some pounding mills used wooden hammers with ends strapped in metal (possibly iron) so the danger cannot be catastrophic.

There has been some confusion amongst today’s craft dyers about exactly which part of the root contains the dyestuff. Nowhere in the book does the author note the differentiation of root into ‘true roots’ and ‘underground stems’ or rhizomes, although some of the quotes from historical documents do allude to this. The root is invariably described as having a thick tough bark but this is clearly an impression formed by looking at the dried root. The skin of fresh root is very thin and can be easily scrubbed away on an individual root but this is probably not possible on a large scale without losing a lot of the underlying dyestuff. The position of the dyestuff in the root is usually described as being just above the woody cortex, but again this is probably a description of a dried root where the soft fleshy outer material has shrunk to a thin layer of concentrated dye bearing material just covering the woody cortex.

Rubia tinctorumIn the shrinking process, the outer skin wrinkles up and appears to become quite thick.

In theory it would be possible to hand wash fresh roots then pound the roots in a strong pan until the woody cores could be removed and the remainder left to dry. This would be very labour intensive however and the inner pith from root stems (which also contains dyestuff) would remain in the removed woody material.

During a Turkey Red workshop run by Debbie Bamford (The Mulberry Dyer) at the 2013 Spinners Weavers and Dyers Guild summer school an experiment was done to try and separate the outer part of the root from the inner cortex and test the resulting material for dye strength and colour. Most of the commercially obtained dried root was actually root stem with the characteristic central dot of red pith. The outer layer of bark and inner dye-rich material was shaved off with potato peelers, down to the pale woody cortex. It was not possible to remove all the dark material. Equal weights of shavings and inner cortex were then used in identical dye baths. The shavings gave the darkest red with little if any dulling due to the presence of outer bark.
root-experiment

For the home dyer wanting the brightest reds the easiest way to remove the brown dyestuffs from the bark is to set up the dye bath using your preferred recipes and after a first heating of root pour off the liquor and replace with fresh water. (See Jenny Dean)

Refining the powdered madder root

When the Madder industry expanded in the 18th and 19th centuries it was not long before competitive manufacturers began to invent new mechanised ways of refining the krap to increase its quality. The first breakthrough using a complex chemical treatment resulted in “garancine” which was later purified even further into “flowers of madder” which was almost pure “alizarin” (the main dye chemical in madder root). These refined products enabled the dyer to dye product quickly, easily and reliably.  Krap became an inferior grade product and perhaps contributed to its entry into the dictionary as the word “crap” meaning rubbish.

For the home dyer, refined madder root products are still produced and sold as madder extracts but these are expensive and I think less exciting than growing your own or making do with chopped root or krap. Home refining is possible (see Michel Garcia) but you do need some specialist laboratory equipment.

Economics

Chenciner is particularly interested in the economics of madder growing, processing and use. As a very high value product, madder growing attracted “adventurer farmers”. It is hard today to imagine farmers being put into the same class as gold prospectors but the potential returns on investment were such that many amateurs were drawn in. Of course many of these inexperienced adventurers were doomed to failure. What seemed like a shortcut to riches and fortune soon turned into a nightmare as old seeds sold by unscrupulous traders failed to germinate or the crop simply failed to grow well or any number of other disasters befell the hapless farmer.

Recipes from History

Contained in the text are numerous recipes for the processing of madder and dyeing of various fibres and textiles. These recipes are often quoted without interpretation into modern terminology so often remain obscure. However, they do offer a fascinating window into historical techniques and a platform for modern attempts to duplicate them.

Historical texts referred to:

The Leyden and Stockholm papyri (a Greek/Egyptian document written around 300AD which contains many recipes for the dyeing of fibre some of which use madder), e.g. :-

  1. Dyeing in Rose Colour  Rose colour is dyed in the following way. Smear the rolls of wool with ashes, untie them, and wash the wool in the liquid from potter’s clay. Rinse it out and mordant it as previously described. Rinse it out in salt water after mordanting and use rain water (which is so) warm that you cannot put your hand in it. Then take for each mina of wool a quarter of a mina of roasted and finely pulverized madder and a quarter of a choenix of bean meat. Mix these together by the addition of white oil, pour it into the kettle and stir up. Put the wool in the kettle and again stir incessantly so that it becomes uniform. When it appears to you to have absorbed the dye liquor, however, brighten it by means of alum, rinse it out again in salt water, and dry it in the shade with protection from smoke.

The Plictho of Gionaventura Rosetti: Instructions in the Art of the Dyers Which Teaches the Dyeing of Woolen Cloths, Linens, Cottons, And Silk by the Great Art As Well as by the Common (1548)

RED Madder wool-spinning-small